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GCMS calibration results for multiple compounds, Dec 2001

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Laboratory report detailing GCMS calibration analysis for various organic compounds including nitrosamines and chlorobenzenes conducted on December 13, 2001.

NYC-WTC_000036498–000036502

Folder label: “GCMS X 12/6/01 A 12/12/01 - 12/13/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\DEC1301\REF.D Vial: 5 Acq On : 13 Dec 2001 1:45 pm Operator: 209 GALOS Sample : gems scan 12/6 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Dec 13 14:34 2001 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Nov 28 15:06:24 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 22.59 168 168682 3.00 ug/1 # 91 31) 4-Bromophenyl-phenylether 23.66 248 92412 2.97 ug/1 96 32) Hexachlorobenzene 24.07 284 96435 2.82 ug/1 99 3 3) Phenanthrene 25.04 178 556095 3.32 ug/1 99 34) Anthracene 25.17 178 502414 3.01 ug/1 99 35) Di-n-butylphthalate 26.98 149 752406 3.37 ug/1 99 36) Fluoranthene 28.65 202 524557 3.24 ug/1 98 3 9) Pyrene 29.31 202 538617 3.04 ug/1 99 40) Butylbenzylphthalate 31.49 149 240755 2.60 ug/1 89 41) Benzo(a)anthracene 32.96 228 390018 3.19 ug/1 100 42) Bis(2-ethylhexyl)phthalate 33.29 149 335785 2.69 ug/1 100 43) Chrysene 33.08 228 431831 3.60 ug/1 99 45) Di-n-Octylphthalate 35.03 149 374324 1.99 ug/1 # 93 46) Benzo(b)fluoranthene 36.03 252 352127 3.31 ug/1 99 4 7) Benzo(k)fluoranthene 36.10 252 404517 3.71 ug/1 99 48) Benzo(a)pyrene 36.92 252 250991 2.71 ug/1 99 49) Indeno(l,2,3-cd)pyrene 40.77 276 248031 2.68 ug/1 94 50) Dibenz(a,h)anthracene 40.84 278 212820 2.94 ug/1 95 51) Benzo(g,h,i)perylene 41.86 276 224313 2.84 ug/1 94

(#) = qualifier out of range (m) = manual integration REF.D GCMS1126.M Fri Dec 21 13:00:53 2001 Page 2

NYC-WTC_000036501

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NYC-WTC_000036501Source: NYC Law Department, mirrored locally

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