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GCMS reference standard analysis results for sample AD29565, Dec 2001

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Laboratory report of GCMS reference standard analysis for sample AD29565 conducted on December 15, 2001.

NYC-WTC_000037099–000037103

Folder label: “GCMS X 12/10/01 A 12/15/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\DEC14 01\REFD.D Vial: 15 Acq On : 15 Dec 2001 4:12 pm Operator: 209 GALOS Sample : gems scan 12/10 a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Dec 15 17:00 2001 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Dec 14 12:19:30 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 22.60 168 122612 3.18 ug/1 # 94 31) 4-Bromophenyl-phenylether 23.65 248 84638 3.97 ug/1 96 3 2) Hexachlorobenzene 24.08 284 97372 4.15 ug/1 97 3 3) Phenanthrene 25.04 178 473018 4.12 ug/1 98 3 4) Anthracene 25.17 178 432786 3.78 ug/1 98 35) Di-n-butylphthalate 26.99 149 684291 4.47 ug/1 99 36) Fluoranthene 28.65 202 444808 4.01 ug/1 97 3 9) Pyrene 29.32 202 457729 3.85 ug/1 99 40) Butylbenzylphthalate 31.49 149 207159 3.34 ug/1 90 41) Benzo(a)anthracene 32.95 228 316278 3.85 ug/1 99 42) Bis(2-ethylhexyl)phthalate 33.29 149 277599 3.31 ug/1 99 43) Chrysene 33.08 228 344159 4.28 ug/1 99 45) Di-n-Octylphthalate 35.03 149 295581 2.43 ug/1 # 89 46) Benzo(b)fluoranthene 36.04 252 290048 4.20 ug/1 99 47) Benzo(k)fluoranthene 36.09 252 327515 4.63 ug/1 100 48) Benzo(a)pyrene 36.93 252 199662 3.33 ug/1 97 4 9) Indeno(1,2,3-cd)pyrene 40.79 276 177382 2.96 ug/1 94 50) Dibenz(a,h)anthracene 40.85 278 145978 3.11 ug/1 97 51) Benzo(g,h,i)perylene 41.87 276 159416 3.11 ug/1 92

(#) = qualifier out of range (m) = manual integration REFD.D GCMS1126.M Fri Dec 28 12:49:46 2001 Page 2

NYC-WTC_000037102

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NYC-WTC_000037102Source: NYC Law Department, mirrored locally

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