GCMS reference standard analysis results for sample AD29565, Dec 2001

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Quantitation Report (QT Reviewed)

Data File : C: \HPCHEM\ 1 \DATA\DEC14 01 \REFD. D Vial: 15 Acq On : 15 Dec 2001 4:12 pm Operator: 209 GALOS Sample : gems scan 12/10 a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Dec 15 17:00 2001 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Dec 14 12:19:30 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) l,4-Dichlorobenzene-d4 11.67 152 787173 20.00 ug/1 -0.02 10) Naphthalene-d8 15.27 136 3033604 20.00 ug/1 -0.03 17) Acenaphthene-diO 20.55 164 1532439 20.00 ug/1 -0.02 29) Phenanthrene-diO 24.98 188 2169896 20.00 ug/1 -0.01 38) Chrysene-dl2 33.01 240 1377487 20.00 ug/1 -0.02 44) Perylene-dl2 37.10 264 917039 20.00 ug/1 -0.01

System Monitoring Compounds 37) 2,4-DDD 30.05 235 168072 5.35 ug/mL -0.02 Spiked Amount 5.000 Recovery = 107.00%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.40 74 75080 2.17 ug/1 88 3) bis(2-Chloroethyl)ether 11.10 93 201283 3.70 ug/1 94 4) 1,3-Dichiorobenzene 11.57 146 137753 2.41 ug/1 99 5) 1,4-Dichlorobenzene 11.57 146 137753 2.38 ug/1 98 6) 1,2-Dichlorobenzene 12.23 146 147667 2.77 ug/1 97 7) 2,2'-oxybis(1-Chioropropan 12.57 45 318796 4.61 ug/1 # 90 8) N-Nitroso-di-n-propylamine 12.96 70 132676 4.29 ug/1 97 9) Hexachloroethane 13.06 117 44123 2.10 ug/1 95 11) Nitrobenzene 13.35 77 169177 3.58 ug/1 92 12) 1sophorone 14.00 82 375870 4.13 ug/1 95 13) bis(2-Chloroethoxy)methane 14.69 93 233269 3.81 ug/1 99 14) 1,2,4-Trichlorobenzene 15.17 180 130296 2.96 ug/1 98 15) Naphthalene 15.33 128 528680 3.65 ug/1 99 16) Hexachlorobutadiene 15.88 225 49609 2.31 ug/1 99 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 18.83 162 299700 3.43 ug/1 97 20) Dimethylphthalate 19.94 163 393224 3.86 ug/1 99 21) 2,6-Dinitrotoluene 20.15 165 63331 2.63 ug/1 # 61 22) Acenaphthylene 20.08 152 459559 3.74 ug/1 100 2 3) Acenaphthene 20.64 153 338767 ’ 3.86 ug/1 99 24) 2,4-Dinitrotoluene 21.32 165 73395 2.40 ug/1 # 87 25) Diethylphthalate 22.07 149 399720 4.24 ug/1 99 26) 4-Chlorophenyl-phenylether 22.20 204 166185 4.04 ug/1 97 2 7) Fluorene 22.16 166 357376 3.96 ug/1 99 2 8) Azobenzen/ 1,2-Diphenylhyd 22.66 77 352583 3.62 ug/L 93

(#) = qualifier out of range (m) = manual integration REFD.D GCMS1126.M Fri Dec 28 12:49:42 2001 Page 1

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