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GCMS reference standard analysis results, Dec 2001

Machine-extracted title · confidence 95%

Laboratory report of GCMS reference standard analysis for sample AD29665 conducted on December 15, 2001.

NYC-WTC_000036967–000036971

Folder label: “GCMS X 12/10/01 A 12/15/01

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\DEC14 01\REFC.D Vial: 4 Acq On : 15 Dec 2001 5:27 am Operator: 209 GALOS Sample : gems scan 12/10 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Dec 28 12:59 2001 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Dec 14 12:19:30 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 22.59 168 127536 3.56 ug/1 # 88 31) 4-Bromophenyl-phenylether 23.66 248 76286 3.85 ug/1 99 32) Hexachlorobenzene 24.07 284 82415 3.78 ug/1 98 3 3) Phenanthrene 25.04 178 446294 4.18 ug/1 99 3 4) Anthracene 25.17 178 391957 3.68 ug/1 99 35) Di-n-butylphthalate 26.98 149 645817 4.55 ug/1 # 98 36) Fluoranthene 28.65 202 415996 4.04 ug/1 99 3 9) Pyrene 29.32 202 433046 3.86 ug/1 98 40) Butylbenzylphthalate 31.49 149 190175 3.25 ug/1 87 41) Benzo(a)anthracene 32.96 228 306190 3.96 ug/1 98 42) Bis(2-ethylhexyl)phthalate 33.29 149 270669 3.42 ug/1 99 43) Chrysene 33.08 228 346094 4.56 ug/1 99 45) Di-n-Octylphthalate 35.03 149 256361 2.27 ug/1 # 92 4 6) Benzo(b)fluoranthene 36.03 252 258322 4.03 ug/1 98 47) Benzo(k)fluoranthene 36.10 252 313885 4.78 ug/1 98 48) Benzo(a)pyrene 36.93 252 188913 3.39 ug/1 98 49) Indeno (1,2,3-cd) pyrene 40.78 276 168679 3.03 ug/1 93 5 0) Dibenz(a,h)anthracene 40.85 278 144961 3.33 ug/1 96 51) Benzo(g,h,i)perylene 41.87 276 151025 3.18 ug/1 91

(#) = qualifier out of range (m) = manual integration REFC.D GCMS1126.M Wed Jan 02 09:13:46 2002 Page 2

NYC-WTC_000036970

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NYC-WTC_000036970Source: NYC Law Department, mirrored locally

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