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GCMS reference material results, Dec 2001

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Laboratory report documenting gas chromatography-mass spectrometry reference material analysis conducted on December 31, 2001.

NYC-WTC_000017658–000017662

Folder label: “GCMS X 12/13/01 A 12/27/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\DEC3101\REF.D Vial: 4 Acq On : 31 Dec 2001 1:53 pm Operator: 209 GALOS Sample : gems scan 12/13 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Jan 7 13:19 2002 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Dec 28 15:11:00 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

.Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 22.61 168 125488 2.85 ug/1 # 31) 4-Bromophenyl-phenylether 23.66 248 100826 4.13 ug/1 32) Hexachlorobenzene 24.08 284 120072 4.47 ug/1 3 3) Phenanthrene 25.05 178 558274 4.25 ug/1 34) Anthracene 25.18 178 510766 3.90 ug/1 35) Di-n-butylphthalate 27.00 149 850019 4.86 ug/1 # 36) Fluoranthene 28.67 202 520475 4.10 ug/1 3 9) Pyrene 29.34 202 537992 4.31 ug/1 97 40) Butylbenzylphthalate 31.50 149 220757 3.39 ug/1 # 81 41) Benzo(a)anthracene 32.97 228 330002 3.83 ug/1 100 42) Bis(2-ethylhexyl)phthalate 33.29 149 300589 3.42 ug/1 96 43) Chrysene 33.09 228 399735 4.74 ug/1 97 45) Di-n-Octylphthalate 35.04 149 301684 2.78 ug/1 # 87 46) Benzo(b)fluoranthene 36.06 252 252207 4.10 ug/1 98 47) Benzo(k)fluoranthene 36.11 252 329932 5.23 ug/1 99 4 8) Benzo(a)pyrene 36.95 252 174809 3.27 ug/1 94 49) Indeno(l,2,3-cd)pyrene 40.87 276 154410 2.89 ug/1 # 89 50) Dibenz(a,h)anthracene 40.92 278 127867 3.05 ug/1 # 92 51) Benzo(g,h,i)perylene 41.93 276 146755 3.21 ug/1 # 90

(#) = qualifier out of range (m) = manual integration REF.D GCMS1126.M Mon Jan 07 13:21:30 2002 Page 2

NYC-WTC_000017661

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NYC-WTC_000017661Source: NYC Law Department, mirrored locally

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