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GCMS analysis results for sample AD29522, Jan 2002

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GCMS analysis report for sample AD29522 listing specific contaminants and surrogate recovery data from January 3, 2002.

NYC-WTC_000036707–000036711

Folder label: “GCMS X 12/7/01 A 1/2/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C: \HPCHEM\ 1 \DATA\DEC3101 \REFF. D Vial: 60 Acq On 3 Jan 2002 12:06 am Operator: 209 GALOS Sample gems scan 12/7 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Jan 16 11:39 2002 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Dec 28 15:11:00 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 22.60 168 169173 2.36 ug/1 # . 78 31) 4-Bromophenyl-phenylether 23.67 248 90994 2.30 ug/1 91 32} Hexachlorobenzene 24.08 284 97161 2.23 ug/1 95 3 3) Phenanthrene 25.04 178 556970 2.61 ug/1 98 34) Anthracene 25.18 178 496908 2.34 ug/1 99 35) Di-n-butylphthalate 27.00 149 807082 2.84 ug/1 # 98 36) Fluoranthene 28.67 202 556211 2.70 ug/1 94 39) Pyrene 29.34 202 556227 2.35 ug/1 97 40) Butylbenzylphthalate 31.50 149 241917 1.96 ug/1 # 80 41) Benzo(a)anthracene 32.98 228 382703 2.35 ug/1 99 42) Bis(2-ethylhexyl)phthalate 33.30 149 323915 1.94 ug/1 98 43) Chrysene 33.10 228 455628 2.85 ug/1 98 45) Di-n-Octylphthalate 35.03 149 343650 1.59 ug/1 # 86 46) Benzo(b)fluoranthene 36.05 252 310321 2.54 ug/1 98 47) Benzo(k)fluoranthene 36.12 252 379455 3.03 ug/1 98 4 8) Benzo(a)pyrene 36.94 252 210206 1.98 ug/1 98 49) Indeno(l,2,3-cd)pyrene 40.86 276 190956 1.80 ug/1 94 5 0) Dibenz(a,h)anthracene 40.93 278 158970 1.91 ug/1 95 51) Benzo(g,h,i)perylene 41.94 276 195464m 2.15 ug/1

(#) = qualifier out of range (m) = manual integration REFF.D GCMS1126.M Wed Jan 16 11:40:04 2002 Page 2

NYC-WTC_000036710

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NYC-WTC_000036710Source: NYC Law Department, mirrored locally

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