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GCMS reference results for sample AD30705, Jan 2002

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Laboratory report documenting GCMS reference analysis of sample AD30705 conducted on January 2, 2002.

NYC-WTC_000018583–000018587

Folder label: “GCMS X 12/19/01 A 1/2/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\1\DATA\DEC31O1\REFE .D Vial: 41 Acq On 2 Jan 2002 3:41 am Operator: 209 GALOS Sample gems scan 12/19a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Jan 25 9:32 2002 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Tue Jan 22 11:56:23 2002 Response via : Initial Calibration DataAcq Meth : GCMS1126

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 22.60 168 128963 2.27 ug/1 97 31) 4-Bromophenyl-phenylether 23.67 248 108930 3.47 ug/1 98 32) Hexachlorobenzene 24.08 284 126257 3.66 ug/1 99 3 3) Phenanthrene 25.04 178 631045 3.73 ug/1 99 3 4) Anthracene 25.18 178 580223 3.44 ug/1 99 35) Di-n-butylphthalate 27.00 149 861612 3.83 ug/1 99 36) Fluoranthene 28.67 202 577821 3.54 ug/1 99 3 9) Pyrene 29.34 202 602199 3.75 ug/1 97 40) Butylbenzylphthalate 31.51 149 267378 3.18 ug/1 97 41) Benzo(a)anthracene 32.97 228 398825 3.59 ug/1 98 42) Bis(2-ethylhexyl)phthalate 33.30 149 356987 3.15 ug/1 99 43) Chrysene 33.09 228 471226 4.33 ug/1 99 45) Di-n-Octylphthalate 35.04 149 383563 2.53 ug/1 95 46) Benzo(b)fluoranthene 36.05 252 321524 3.74 ug/1 99 47) Benzo(k)fluoranthene 36.11 252 405986 4.60 ug/1 98 4 8) Benzo(a)pyrene 36.95 252 234748 3.14 ug/1 97 49) Indeno(1,2,3-cd) pyrene 40.85 276 215965 2.89 ug/1 # 92 5 0) Dibenz(a,h)anthracene 40.92 278 177137 3.03 ug/1 95 51) Benzo(g,h,i)perylene 41.92 276 190530 2.99 ug/1 98

(#) = qualifier out of range (m) = manual integration REFE.D GCMS1126.M Fri Jan 25 09:36:38 2002 Page 2

NYC-WTC_000018586

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NYC-WTC_000018586Source: NYC Law Department, mirrored locally

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