GCMS reference results for sample AD30705, Jan 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\1\DATA\DEC3101\REFE.D Vial: 41 Acq On 2 Jan 2002 3:41 am Operator: 209 GALOS Sample gems scan 12/19a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Jan 25 9:32 2002 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title ■: 209 625/TCLP calibration table Last Update : Tue Jan 22 11:56:23 2002 Response via : Initial Calibration DataAcq Meth : GCMS1126

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) l,4-Dichlorobenzene-d4 11.67 152 1126402 20.00 ug/1 -0.03 10) Naphthalene-d8 15.27 136 4320283 20.00 ug/1 -0.03 17) Acenaphthene-diO 20.55 164 2140016 20.00 ug/1 -0.02 29) Phenanthrene-diO 24.98 188 3193165 20.00 ug/1 -0.01 38) Chrysene-dl2 33.02 240 1862284 20.00 ug/1 -0.01 44) Perylene-dl2 37.11 264 1141880 20.00 ug/1 0.00

System Monitoring Compounds 37) 2,4-DDD 30.06 235 176932 5.04 ug/mL 0.00 Spiked Amount 5.000 Recovery = 100.80%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.32 74 8,7724 1.77 ug/1 88 3) bis(2-Chloroethyl)ether 11.09 93 271300 3.49 ug/1 99 4) 1,3-Dichiorobenzene 11.57 146 166980 2.04 ug/1 100 5) 1,4-Dichlorobenzene 11.71 146 184257 2.22 ug/1 ‘98 6) 1,2-Dichlorobenzene 12.23 146 185779 2.43 ug/1 96 7) 2,2'-oxybis(1-Chloropropan 12.56 45 466483 4.71 ug/1 # 93 8) N-Nitroso-di-n-propylamine 12.94 70 192807 4.35 ug/1 99 9) Hexachloroethane 13.05 117 50441 1.67 ug/1 97 11) Nitrobenzene 13.36 77 238379 3.54 ug/1 98 12) Isophorone 14.00 82 534122 4.12 ug/1 100 13) bis(2-Chloroethoxy)methane 14.69 93 313691 3.60 ug/1 99 14) 1,2,4-Trichlorobenzene 15.17 180 155966 2.49 ug/1 98 15) Naphthalene 15.33 128 675070 3.27 ug/1 100 16) Hexachlorobutadiene 15.88 225 45267 1.48 ug/1 95 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 18.85 162 364741 2.99 ug/1 98 20) Dimethylphthalate 19.95 163 536243 3.77 ug/1 100 21) 2,6-Dinitrotoluene 20.16 165 83767 2.49 ug/1 94 2 2) Acenaphthylene 20.09 152 563999 3.29 ug/1 100 2 3) Acenaphthene 20.64 153 433978 3.54 ug/1 ■ 99 24) 2,4-Dinitrotoluene 21.35 165 88393 2.07 ug/1 91 25) Diethylphthalate 22.07 149 571384 4.34 ug/1 99 26) 4-Chlorophenyl-phenylether 22.21 204 209057 3.64 ug/1 98 27) Fluorene 22.17 166 458389 3.64 ug/1 99 28) Azobenzen/ 1,2-Diphenylhyd 22.66 77 588117 4.33 ug/L 94

(#) = qualifier out of range (m) = manual integration REFE.D GCMS1126.M Fri Jan 25 09:36:34 2002 Page 1

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