GCMS calibration results for multiple compounds, Dec 2001

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\DEC1301\REF.D Vial: 5 Acq On : 13 Dec 2001 1:45 pm Operator: 209 GALOS Sample : gems scan 12/6 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Dec 13 14:34 2001 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Nov 28 15:06:24 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 11.67 152 1145194 20.00 ug/1 -0.03 10) Naphthalene-d8 15.28 136 4362802 20.00 ug/1 -0.03 17) Acenaphthene-diO 20.56 164 2168885 20.00 ug/1 -0.02 29) Phenanthrene-diO 24.98 188 3166546 20.00 ug/1 -0.01 38) Chrysene-dl2 33.01 240 2050909 20.00 ug/1 -0.02 44) Perylene-dl2 37.10 264 1414042 20.00 ug/1 -0.02

System Monitoring Compounds 37) 2,4-DDD 30.05 235 166349 4.41 ug/mL -0.02 Spiked Amount 5.000 Recovery = 88.20%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.40 74 102927 2.04 ug/1 90 3) bis(2-Chloroethyl)ether 11.10 93 240261 3.04 ug/1 95 4) 1,3-Dichlorobenzene 11.58 146 136849 1.64 ug/1 97 5) 1,4-Dichlorobenzene 11.58 146 136849 1.62 ug/1 98 6) 1,2-Dichlorobenzene 12.23 146 152341 1.96 ug/1 98 7) 2,2'-oxybis(1-Chloropropan 12.57 45 365702 3.63 ug/1 # 91 8) N-Nitroso-di-n-propylamine 12.95 70 163313 3.63 ug/1 96 9) Hexachloroethane 13.06 117 36958 1.21 ug/1 97 11) Nitrobenzene 13.35 77 204661 3.01 ug/1 89 12) 1sophorone 14.00 82 457621 3.49 ug/1 97 13) bis(2-Chloroethoxy)methane 14.69 93 282973 3.22 ug/1 99 14) 1,2,4-Trichlorobenzene 15.17 180 126501 2.00 ug/1 98 15) Naphthalene 15.33 128 562871 2.70 ug/1 99 16) Hexachlorobutadiene 15.88 225 32508 1.05 ug/1 94 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 18.82 162 318328 2.57 ug/1 98 20) Dimethylphthalate 19.93 163 475791 3.30 ug/1 100 21) 2,6-Dinitrotoluene 20.14 165 81178 2.38 ug/1 # 62 22) Acenaphthylene 20.09 152 497257 2.86 ug/1 99 23) Acenaphthene 20.64 153 362884 2.92 ug/1 99 24) 2,4-Dinitrotoluene 21.32 165 96455 2.23 ug/1 # 85 25) Diethylphthalate 22.06 149 471129 3.53 ug/1 98 26) 4-Chlorophenyl-phenylether 22.20 204 177130 3.04 ug/1 99 27) Fluorene 22.16 166 400451 3.14 ug/1 97 28) Azobenzen/ 1,2-Diphenylhyd 22.66 77 462560 3.36 ug/L 94

(#) = qualifier out of range (m) = manual integration REF.D GCMS1126.M Fri Dec 21 13:00:49 2001 Page 1

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