GCMS reference standard results for sample AD29926, Jan 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\l\DATA\DEC1401\REF.D Vial: 42 Acq On : 16 Dec 2001 6:45 am Operator: 209 GALOS Sample : gems scan 12/11 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Jan 30 10:13 2002 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Jan 25 15:57:52 2002 Response via : Initial Calibration DataAcq Meth : GCMS1126

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 11.67 152 804781 20.00 ug/1 -0.03 10) Naphthalene-d8 15.28 136 3117633 20.00 ug/1 -0.03 17) Acenaphthene-dlO 20.55 164 1534565 20.00 ug/1 -0.03 29) Phenanthrene-diO 24.97 188 2211664 20.00 ug/1 -0.02 38) Chrysene-dl2 33.01 240 1416698m 20.00 ug/1 -0.03 44) Perylene-dl2 37.10 264 933188 20.00 ug/1 -0.02

System Monitoring Compounds 37) 2,4-DDD 30.05 235 114911 4.73 ug/mL -0.02 Spiked Amount 5.000 Recovery = 94.60%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.40 74 74107 2.09 ug/1 95 3) bis(2-Chloroethyl)ether 11.10 93 181722 3.27 ug/1 95 4) 1,3-Dichlorobenzene 11.57 146 102815 1.76 ug/1 98 5) 1,4-Dichlorobenzene 11.57 146 102815 1.74 ug/1 97 6) 1,2-Dichlorobenzene 12.23 146 117916 2.16 ug/1 95 7) 2,2'-oxybi s(1-Chioropropan 12.57 45 290686 4.11 ug/1 94 8) N-Nitroso-di-n-propylamine 12.96 70 123222 3.89 ug/1 96 9) Hexachloroethane 13.07 117 29161 1.35 ug/1 100 11) Nitrobenzene 13.36 77 154137 3.17 ug/1 99 12) Isophorone 14.00 82 343561 3.67 ug/1 98 13) bis(2-Chloroethoxy)methane 14.69 93 207000 3.29 ug/1 98 14) 1,2,4-Trichlorobenzene 15.17 180 99284 2.19 ug/1 99 15) Naphthalene 15.33 128 443069 2.97 ug/1 99 16) Hexachlorobutadiene 15.89 225 28082 1.27 ug/1 98 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 18.83 162 242638 2.77 ug/1 96 20) Dimethylphthalate 19.93 163 342159 3.36 ug/1 99 21) 2,6-Dinitrotoluene 20.14 165 54280 2.25 ug/1 98 22) Acenaphthylene 20.09 152 375739 3.05 ug/1 99 23) Acenaphthene 20.64 153 284795 3.24 ug/1 98 24) 2,4-Dinitrotoluene 21.33 165 63336 2.07 ug/1 91 25) Diethylphthalate 22.06 149 359388 3.81 ug/1 98 26) 4-Chlorophenyl-phenylether 22.20 204 135048 3.28 ug/1 94 27) Fluorene 22.16 166 297435 3.29 ug/1 97 28) Azobenzen/ 1,2-Diphenylhyd 22.66 77 301641 3.09 ug/L 98

(#) = qualifier out of range (m) = manual integration REF.D GCMS1126.M Wed Jan 30 10:14:44 2002 Page 1

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