GCMS reference data for sample AD30694, Jan 2002

NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\1\DATA\DEC3101\REFD.D Vial: 27 Acq On 1 Jan 2002 2:08 pm Operator: 209 GALOS Sample gems scan 12/19 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Jan 18 8:43 2002 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update • : Fri Dec 28 15:11:00 2 001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 11.68 152 979210 20.00 ug/1 -0.02 10) Naphthalene-d8 15.28 136 3789979 20.00 ug/1 -0.02 17) Acenaphthene-dlO 20.56 164 1891860 20.00 ug/1 -0.01 29) Phenanthrene-diO 24.98 188 2862295m 20.00 ug/1 -0.01 38) Chrysene-dl2 33.02 240 1807168 20.00 ug/1 -0.01 44) Perylene-dl2 37.12 264 1050070 20.00 ug/1 0.00

System Monitoring Compounds 37) 2,4-DDD 30.06 235 162455 5.16 ug/mL 0.00 Spiked Amount 5.000 Recovery = 103.20%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.43 74 106572 2.47 ug/1 # 69 3) bis(2-Chloroethyl)ether 11.10 93 263721m 3.90 ug/1 4) 1,3-Dichlorobenzene 11.58 146 164989 2.32 ug/1 97 5) 1,4-Dichlorobenzene 11.72 146 187672 2.61 ug/1 # 97 6) 1,2-Dichlorobenzene 12.24 146 185841 2.80 ug/1 99 7) 2,2'-oxybi s(1-Chloropropan 12.57 45 461602 5.36 ug/1 # 91 8) N-Nitroso-di-n-propylamine 12.96 70 191685 4.98 ug/1 90 9) Hexachloroethane 13.06 117 51016 1.95 ug/1 95 11) Nitrobenzene 13.37 77 241887 4.09 ug/1 # 84 12) 1sophorone 14.00 82 519591 4.57 ug/1 # 92 13) bis(2-Chloroethoxy)methane 14.70 93 296302 3.88 ug/1 98 14) 1,2,4-Trichlorobenzene 15.17 180 156295 2.84 ug/1 98 15) Naphthalene 15.34 128 665937 3.68 ug/1 99 16) Hexachlorobutadiene 15.89 225 43136 1.61 ug/1 97 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 18.85 162 363442 3.37 ug/1 95 20) Dimethylphthalate 19.95 163 487632 3.88 ug/1 99 21) 2,6-Dinitrotoluene 20.16 165 82226 2.77 ug/1 # 58 2 2) Acenaphthylene 20.09 152 559184 3.69 ug/1 99 23) Ac enapht hene 20.65 153 419019 3.86 ug/1 100 24) 2,4-Dinitrotoluene 21.35 165 85075 2.25 ug/1 # 61 25) Diethylphthalate 22.07 149 514939 4.43 ug/1 98 26) 4-Chlorophenyl-phenylether 22.21 204 197652 3.89 ug/1 95 27) Fluorene 22.17 166 440491 3.96 ug/1 99 28) Azobenzen/ 1,2-Diphenylhyd 22.67 77 525220 4.37 ug/L # 84

(#) = qualifier out of range (m) = manual integration REFD.D GCMS1126.M Fri Jan 18 08:44:02 2002 Page 1

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