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GCMS reference analysis results for sample AD31586, January 2002

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Laboratory report of GCMS reference analysis for sample AD31586 listing chemical standards and response values.

NYC-WTC_000049679–000049683

Folder label: “GCMS X 1/2/02 A 1/3 - 1/4/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\1\DATA\JAN03 02\REFB.D Vial: 32 Acq On 4 Jan 2002 4:44 pm Operator: 209 GALOS Sample gems scan 1/2a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Feb 1 9:31 2002 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Tue Jan 22 11:56:23 2002 Response via : Initial Calibration DataAcq Meth : GCMS1126

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 22.43 168 103869 2.81 ug/1 99 31) 4-Bromophenyl-phenylether 23.49 248 71548 3.49 ug/1 98 3 2) Hexachlorobenzene 23.91 284 78175 3.47 ug/1 99 3 3) Phenanthrene 24.87 178 415229 3.77 ug/1 99 34) Anthracene 25.00 178 371804 3.38 ug/1 99 35) Di-n-butylphthalate 26.83 149 597397 4.07 ug/1 99 36) Fluoranthene 28.48 202 386631 3.63 ug/1 98 39) Pyrene 29.14 202 399085 3.68 ug/1 99 40) Butylbenzylphthalate 31.33 149 169607 3.00 ug/1 99 41) Benzo(a)anthracene 32.78 228 259052 3.46 ug/1 99 42) Bis(2-ethylhexyl)phthalate 33.13 149 209235 2.74 ug/1 99 43) Chrysene 32.90 228 281023 3.83 ug/1 99 45) Di-n-Octylphthalate 34.88 149 207688 2.11 ug/1 # 96 4 6) Benzo(b)fluoranthene 35.86 252 204274 3.66 ug/1 99 47) Benzo(k)fluoranthene 35.92 252 251356 4.39 ug/1 99 4 8) Benzo(a)pyrene 36.73 252 139743 2.88 ug/1 99 49) Indeno(l,2,3-cd)pyrene 40.48 276 142617 2.94 ug/1 96 50) Dibenz(a,h)anthracene 40.54 278 119788 3.16 ug/1 98 51) Benzo(g,h,i)perylene 41.53 276 133364 3.22 ug/1 99

(#) = qualifier out of range (m) = manual integration REFB.D GCMS1126.M Fri Feb 01 09:33:45 2002 Page 2

NYC-WTC_000049682

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NYC-WTC_000049682Source: NYC Law Department, mirrored locally

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