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GCMS calibration results for sample AD30470, Jan 2002

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Laboratory report documenting GCMS calibration data for sample AD30470 conducted on December 31, 2001.

NYC-WTC_000017898–000017902

Folder label: “GCMS X 12/14/01 A 12/31/01

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\DEC3101\REFA.D Vial: 6 Acq On : 31 Dec 2001 3:50 pm Operator: 209 GALOS Sample : gems scan 12/14 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Dec 31 16:38 2001 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update • : Fri Dec 28 15:11:00 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 22.61 168 119856 3.18 ug/1 # 79 31) 4-Bromophenyl-phenylether 23.67 248 75799 3.63 ug/1 # 88 32) Hexachlorobenzene 24.08 284 89481 3.89 ug/1 # 90 3 3) Phenanthrene 25.04 178 446672 3.97 ug/1 99 34) Anthracene 25.18 178 527570 4.70 ug/1 99 35) Di-n-butylphthalate 27.00 149 647450 4.32 ug/1 # 98 3 6) Fluoranthene 28.67 202 446858 4.11 ug/1 98 39) Pyrene 29.34 202 467681 4.16 ug/1 97 40) Butylbenzylphthalate 31.51 149 213103 3.63 ug/1 # 84 41) Benzo(a)anthracene 32.97 228 327460 4.22 ug/1 99 42) Bis(2-ethylhexyl)phthalate 33.30 149 248492 3.13 ug/1 96 43) Chrysene 33.09 228 419625 5.51 ug/1 99 45) Di-n-Octylphthalate 35.04 149 276797 2.70 ug/1 # 87 46) Benzo(b)fluoranthene 36.06 252 245615 4.24 ug/1 99 47) Benzo(k)fluoranthene 36.11 252 341524 5.74 ug/1 98 4 8) Benzo(a)pyrene 36.95 252 184759 3.66 ug/1 96 49) Indeno(1,2,3-cd) pyrene 40.86 276 158085 3.14 ug/1 96 50) Dibenz(a,h)anthracene 40.92 278 134491 3.41 ug/1 # 91 51) Benzo(g,h,i)perylene 41.93 276 149098 3.46 ug/1 92

(#) = qualifier out of range (m) = manual integration REFA.D GCMS1126.M Tue Jan 15 11:14:07 2002 Page 2

NYC-WTC_0000 17901

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NYC-WTC_000017901Source: NYC Law Department, mirrored locally

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