GCMS calibration results for sample AD30470, Jan 2002

NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\l\DATA\DEC3101\REFA.D Vial: 6 Acq On : 31 Dec 2001 3:50 pm Operator: 209 GALOS Sample : gems scan 12/14 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Dec 31 16:38 2001 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update • : Fri Dec 28 15:11:00 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 11.68 152 758271 20.00 ug/1 -0.02 10) Naphthalene-d8 15.28 136 2934290 20.00 ug/1 -0.03 17) Acenaphthene-diO 20.55 164 1506182 20.00 ug/1 -0.02 29) Phenanthrene-diO 24.99 188 2124920 20.00 ug/1 0.00 38) Chrysene-dl2 33.02 240 1302356 20.00 ug/1 -0.01 44) Perylene-dl2 37.12 264 770787 20.00 ug/1 0.00

System Monitoring Compounds 37) 2,4-DDD 30.06 235 119163 5.10 ug/mL 0.00 Spiked Amount 5.000 Recovery = 102.00%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.43 74 82449 2.47 ug/1 # 72 3) bis(2-Chloroethyl)ether 11.11 93 189578 3.62 ug/1 92 4) 1,3-Dichlorobenzene 11.58 146 117896 2.14 ug/1 97 5) 1,4-Dichlorobenzene 11.72 146 138687 2.49 ug/1 # 97 6) 1,2-Dichiorobenzene 12.24 146 138709 2.70 ug/1 99 7) 2,2'-oxybi s(1-Chioropropan 12.58 45 341837 5.13 ug/1 # 91 8) N-Nitroso-di-n-propylamine 12.97 70 134935 4.53 ug/1 # 87 9) Hexachloroethane 13.06 117 33252 1.64 ug/1 88 11) Nitrobenzene 13.37 77 169465 3.71 ug/1 # 86 12) 1sophorone 14.01 82 369867 4.20 ug/1 # 92 13) bis(2-Chloroethoxy)methane 14.70 93 214927 3.63 ug/1 99 14) 1,2,4-Trichlorobenzene 15.17 180 118731 2.79 ug/1 100 15) Naphthalene 15.34 128 499565 3.56 ug/1 99 16) Hexachlorobutadiene 15.89 225 33308 1.60 ug/1 94 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 18.86 162 267802 3.12 ug/1 95 20) Dimethylphthalate 19.96 163 360048 3.60 ug/1 99 21) 2,6-Dinitrotoluene 20.17 165 51644 2.18 ug/1 # 60 22) Ac enaphthylene 20.09 152 395481 3.27 ug/1 100 2 3) Acenaphthene 20.65 153 308615 3.57 ug/1 100 24) 2,4-Dinitrotoluene 21.38 165 51442 1.71 ug/1 # 70 25) Diethylphthalate 22.08 149 377629 4.08 ug/1 98 26) 4-Chlorophenyl-phenylether 22.21 204 145209 3.59 ug/1 # 90 27) Fluorene 22.17 166 318992 3.60 ug/1 99 28) Azobenzen/ 1,2-Diphenylhyd 22.67 77 369907 3.87 ug/L # 87

(#) = qualifier out of range (m) = manual integration REFA.D GCMS1126.M Tue Jan 15 11:14:03 2002 Page 1

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