Laboratory report noting GCMS scan results for sample AD29231 with phthalates detected and low recovery requiring re-analysis.
NYC-WTC_000036162–000036183Folder label: “GCMS X 12/3/01 A 12/10/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\DEC2701\29231.D Vial: 57 Acq On : 30 Dec 2001 3:05 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/18 A Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title 209 625/TCLP calibration table Library C:\DATABASE\NBS75K.L ******************************************** * *** * ** * *********** * * * * * * Peak Number 5 Cyclopentasiloxane, decamethyl Concentration Rank 4
R.T. EstConc Area Relative to ISTD R.T.
14.30 1.83 ug/1 2332340 Naphthalene-d8 15.30
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Cyclopentasi oxane, decame thyl- 000541-02-6 370 C10H3005Si5 50 2 3,4 -Dihydroxybenzyl alcohol, tris (tr 356 C16H3203Si3 068595-79-9 38 3 Benzoic id, 2,6-bis [ ( trimethylsil 370 C16H30O4Si3 003782-85-2 33 4 Benzeneethanamine, N- [ (pentafluorop 475 C21H26F5NO2Si2 055429-85-1 32 'Abundance Scan 1009 (14.305 min): 29231.D (-) m/z 72.95 100.00% 73
5000 267 355 45 14.00 14.20 14.40 14.60 1 । t 88 103 IIPN 133 154 177 193208223 251 | TTT| . | ! 293 —uugmuurdur 323339 ' i ■ ■ ■' i ■ ! . i | . . . . |Tl ll) iTlTp TT I | m/z 267.00 31.41% miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 'Abundance #51266: Cyclopentasiloxane, decamethyl- 73
355 267 ------ 5000 14.00 14.20 14.40 14.60 m/z 355.05 23.06% 191207 2511 323339 •' । ‘1 ■' । ■ miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #49868: 3,4-Dihydroxybenzyl alcohol, tris(trimethylsilyl)- 73 / TET — 1’1/1/1111 14.00 14.20 14.40 14.60 267 m/z 268.00 8.37% 5000 179 356 45 147 i
209 237 312 341 1 TTOE’TTIII’IIIITIT r • • • i1' • ‘ i " 11 i • • •' r • • • i ‘ “ i ‘ ‘ • r • • • i 111 ■ I ■1 ‘11111' I' miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 'Abundance #51296: Benzoic acid, 2,6-bis[(trimethylsilyl)oxy]-, trimet i ■ ■ ■ ' i ' ' ' ' i 73 355 14.00 14.20 14.40 14.60 m/z 356.05 8.37% 5000
147 267
miz-> 47 ' 'i " ' 40 I "‘‘IT /X 1' 1111 I *1'' I 208 TT n-p-r TTTI i 249 i i " " i TTTT 7 6G 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 2,83 370 ) TIr +... 14.00 14.20 14.40 14.60
29231.D GCMS1126.M Mon Dec 31 13:59:25 2001 Page 5
NYC-WTC_000036172
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