GCMS analysis results for sample AD28471, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Date File C: \HPCHEM\1\DATA\DEC04 01\28471.D vial; 7 Acc On 4 Dec 2001 6:13 pm Operator; 209 GALOS Sample gc/ms 11/24 Inst : GC/MS 209 Mist Multiplr: 1.00 MS integration Params; LSCINT.P Quat Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Tit- e : 209 625/TCLP calibration table Library : C : \DATABASE\NBS75K . L ***** ************** ********************************* * * ************** Peak Cumber 10 Hexatriacontane Concentration Rank 8 R. T EstConc Area Relative to ISTD R.T. 35.4:, 0.89 ug/1 193941 Perylene-dl2 37.13 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Hezatriacontane 507 C36H74 000630-06-8 2 Eicosane 282 C20H42 000112-95-8 3 Tetratetracontane 619 C44H90 007098-22-8 91 4 Pe .tacosane 352 C25H52 000629-99-2 91 Abundanc Scon 3309 (35.424 min): 28471 .D (-) m/z 56.95 100.00% 57

85 500C I TTTT0r0 13141169197225 282 35.00 35.20 35.40 35.60 35.80 " f 1 T i TT "TII—muun Tur । । । । . m/z 43.00 69.86% m/z-> 50 100 150 200 250 300 350 400 450 500 550 600 Abundan . #74636: Hexatriacontane 57

500 | 85 J 35.00 35.20 35.40 35.60 35.80 m/z71.05 66.57% : 1

TIT 113141169197 ............................... m/z—> 50 100 150 200 250 300 350 400 450 500 550 600 Abundance #72324: Eicosane 431 TTTTTr 71 35.00 35.20 35.40 35.60 35.80 5000 m/z 85.05 52.55%

199 — J 1 L 141169197 254282 -....... । । । । , । । ।। ।।। miz-> 50 100 150 200 250 300 350 400 450 500 550 600 Abundance #61068: Tetratetracontane 57 - )0 35.20 35.6 ) I m/z 55.00 27.35% — 5000 ; 85

. ■ 13141169197:25 379407 590618 7 rT T—tmtrr, - . । . . . . । . . . . । . n , । . . . , । 11—1— m/z-> 50 100 150 200 250 300 350 400 450 500 550 600 35,00 35.20 35.40 35,60 35.80

28471 D GCMS1126.M Wed Dec 05 11:27:49 2001 Page 10

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