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GCMS analysis results for sample AD28471, Dec 2001

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Laboratory report documenting GCMS analysis of sample AD28471 conducted on December 6, 2001.

NYC-WTC_000034347–000034365

Folder label: “GCMS X 11/21/01 A 11/27 - 11/28/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Dati File C: \HPCHEM\1\DATA\DEC0401\28471 .D vial: 7 Acc On 4 Dec. 2001 6:13 pm Operator: 209 GALOS Sample gc/ms 11/24 Inst : GC/MS 209 Mis: Multiplr: 1.00 MS integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Lib rary : C:\DATABASE\NBS75K.L ********************************************************************* Peak number 11 Heptadecane Concentration Rank 11 R.T EatCone Area Relative to ISTD R.T. 36.2: 0.41 ug/1 89722 Perylene-dl2 37.13

Hit# of 5 TentEitive ID MW MolForm CAS# Qual

1 Heptadecane 240 C17H36 000629-78-7 96 2 Hexatriacontane 507 C36H74 000630-06-8 91 3 Tetratetracontane 619 C44H90 007098-22-8 91 4 Nonacosane 408 C29H60 000630-03-5 90 Abundanc.. Scan 3403 (36.287 min): 28471 .D (-) m/z 57.00 100.00% 57

85 5000

' ' TTT < । ‘ TTPTTf 36.00 36.20 36.40 36.60 i 1, — 1 110 .17720 253 m/z 43.05 69.60% mz->_ Abundant 2 50 100 150 200 250 300 350 400 #32063: Heptadecane 450 500 550 600 5.7

5001 i |85 36.00 36.20 36.40 36.60 m/z 71.05 65.47% 13 —141196 24- miz-> 50___ 100 150 200 250 300 350 400 450 500 550 600 Abundance #74636: Hexatrlacontane ,57 ACYM 4 41477 TMMAR 4 36.00 36.20 36.40 36.60 m/z 85.05 54.57% 5000

ill mfz-> Abundarc. “T!. H 50 57 ; 113141169197 ,—Th 11 t TTT—" r 100 150 200 250 300 350 400 #74745: Tetratetracontane 450 500 550 600 LAM, AA € 4 A■ ■ i ■ ■ 36.00 36.20 36.40 36.60 m/z 55.00 23.34% . — 5000 85 i " 113141 ................................. 463491519547,591618 m/z—> 50 100 150 200 250 300 350 400 450 500 550 600 36.00 36.20 36.40 3660

28471.D GCMS1126.M Wed Dec 05 11:27:52 2001 Page 11

NYC-WTC_000034364

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NYC-WTC_000034364Source: NYC Law Department, mirrored locally

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