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GCMS analysis results for sample AD28471, Dec 2001

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Laboratory report documenting GCMS analysis of sample AD28471 conducted on December 6, 2001.

NYC-WTC_000034347–000034365

Folder label: “GCMS X 11/21/01 A 11/27 - 11/28/01

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Scanned page image, NYC-WTC_000034362
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NYC 9/11 Public Portal Document

Library Search Compound Report Dat . File C:\HPCHEM\1\DATA\DEC0401\28471.D Vial: 7 Acc On 4 De. 2001 6:13 pm Operator: 209 GALOS Sample gc/ms 11/24 Inst : GC/MS 209 Mis. Multiplr: 1.00 MS integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Tit le : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Jumber 9 Heptadecane Concentration Rank 10 R. T EstConc Area Relative to ISTD R.T. 34.5. 0.84 ug/1 221653 Chrysene-dl2 33.04 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Heptadecane 240 C17H36 000629-78-7 98 2 Heatriacontane 507 C36H74 000630-06-8 3 Pentacosane 352 C25H52 000629-99-2 91 4 Do osane 310 C22H46 000629-97-0 91 Abundanc. Sun 3212 (34.533 min): 28471 .D (-) m/z 57.00 100.00% 57

i , 85 5000 i

1111 m . । । । 34.20 34.40 34.60 34.80 -1111,11,169 197240.................... m/z 71.00 69.74% m/z-> 50 100 150 200 250 300 350 400 450 500 Abundance #32063: Heptadecane 57 : ! 85 500L |ii TTT01—rrponduT 34.20 34.40 34.60 34.80 m/z43.05 68.02% 113 ...

mz-> -L 50 -111 100 150 196 240 ................ 200 250 300 350 400 450 500 Abundanc- #59136: Hexatriacontane 57 . TTTTT 34.20 34.40 34.60 34.80 500C i l m/z 85.05 53.46% i l 85 ! ' 1

JliqluX , 239 ....... 379 407 435 , 478 506 ti/z-> 50 100 150 200 250 300 350 400 450 500 Abundant #73718: Pentacosane i r 1 r (i । r i i । i-T ! i । f i 43 ; 34.20 34.40 34.60 34.80 m/z41.05 / 26.41% i 71 5000 I I

i 124127,155 133 211 4 —TTPM4 m/z—> 50 100 150 200 250 300 350 400 450 500 34.20 34.40 34.60 34.80

28471.D GCMS1126.M Wed Dec 05 11:27:47 2001 Page 9

NYC-WTC_000034362

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NYC-WTC_000034362Source: NYC Law Department, mirrored locally

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