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← Document results/DEP Box 21/GCMS X 11/20/01 A 11/26/01
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GCMS Method 508 calibration data sheet, Nov 2001

Machine-extracted title · confidence 100%

Technical data sheet recording instrument parameters and calibration details for GCMS Method 508 analysis conducted in November 2001.

NYC-WTC_000033886–000033901

Folder label: “GCMS X 11/20/01 A 11/26/01”

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Scanned page image, NYC-WTC_000033892
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C: \HPCHEM\ 1 \DATA\NOV2 6 01 \LBA. D Vial: 9 Acq On : 26 NOV 2001 6:31 pm Operator: 209 GALOS Sample : 11/20 lab bik scan Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 l,4-Dichlorobenzene-d4 Concentration Rank 8

R.T. EstConc Area Relative to ISTD R.T.

11.56 0.51 ug/1 129074 1,4-Dichlorobenzene-d4 11.70 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1,4-Dichlorobenzene-d4 150 C6C12D4 003855-82-1 53 2 Benze: -1,2,3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 25 3 Benzaldehyde, dehyde 2 -hydroxy- 3 -methoxy- 152 C8H803 000148-53-8 10 4 Acenaphthylene 152 C12H8 000208-96-8 10 Abundance Scan 710 (11.560 mln): LBA.D (-) m/z 149.90 100.00% 1$0

5000 115 78 -T—dn—mTTTTTTTTT 52 40 .1,, 63 11.20 11.40 11.60 11.80 mpHH- il 87 99 ympmm ,1TTT—ug—u"guuT 207 m/z 151.90 63.52% miz-?___ 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 Abundance #9593: 1,4-Dichlorobenzene-d4 150

5000- 115 TT T T 78 11.20 11.40 11.60 11.80 52 m/z 114.90 34.97% 35 87 " I" " r "11 ।" r ■ +.....TIT TTTTT "TUIOTEIItTTT TTTTTTTTTTTTTTITT | H l'l | I I I I | I U > | n m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 Abundance 39522; Benzers1,2,3.4-d4-, 5,6-dichloro- 150

115 11.20 11.40 11.60 11.80 5000 52 78 m/z 78.05 19.35%

35 87 UI—T—gumTtgT 11«rt11 >> i ■ । 11 H m m m 4 — mmmmm miz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 Abundance #66892: Benzaldehyde, 2-hydroxy-3-methoxy- 1$2 11.20 11.40 11.60 11.80 m/z 52.00 14.11% 106 5000 53 81

92 122 .. il 136 / miz-> 3040 50/60 70 8090/180 110 720 130140 150 160 170 180 190 200 210 ' 11.20 11.40 11.60 11.80

LBA.D GCMS1126.M Thu Jan 03 12:52:06 2002 Page 1

NYC-WTC_000033892

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