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← Document results/DEP Box 21/GCMS X 11/20/01 A 11/26/01
Document / 16 pages

GCMS blank analysis results for sample AD28143, Nov 2001

Machine-extracted title · confidence 100%

Laboratory report of a GCMS blank analysis for sample AD28143 conducted on November 28, 2001, listing various organic compounds below detection limits.

NYC-WTC_000033707–000033722

Folder label: “GCMS X 11/20/01 A 11/26/01”

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Scanned page image, NYC-WTC_000033713
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C: \HPCHEM\ 1 \DATA\NOV2 601 \LBA. D Vial : 9 Acq On : 26 Nov 2001 6:31 pm Operator : 209 GALOS Sample : 11/20 lab blk scan Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 1,4-Dichlorobenzene-d4 Concentration Rank 8

R.T. EstConc Area Relative to ISTD R.T.

11.56 0.51 ug/1 129074 1,4-Dichlorobenzene-d4 11.70

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1,4-Dichlorobenzene-d4 150 C6C12D4 003855-82-1 53 2 Benzene-1/2,3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 25 3 Benzaldehyde, 2-hydroxy-3-methoxy- 152 C8H803 000148-53-8 10 4 Acenaphthylene 152 C12H8 000208-96-8 10 Abundance Scan 710 (11.560 min): LBA.D (-) m/z 149.90 100.00% 150

5000 115 78 —TI=nn—’—TTTeruTu’Tr 52 11.20 11.40 11.60 11.80 40 . 63 87 99 J1 I | TTTHHH TTT I T th t r’T TTTTT i r n TTT I 1 fl T TTT TTTTT TTTTTTT 207 m/z 151.90 63.52% mz-> 30 40 50 60 70 80 90 100 110 120130 140 150 160 170 180 190 200 210 Abundance #9593:1,4-Dichlorobenzene-d4 150

5000 115 TT—mmmTTTTTETTTT 78 1120 11,40 11.60 11.80 52 m/z 114.90 . 34.97% — 87 mmmm 35 mz-> 30 40 50 60 70 80 90 100 110 120130 140 150 160 170 180 190 200 210 Abundance #9592: Benzene-1,2,3,4-d4-, 5,6-dichloro- 150

115 1120 11.40 11.60 11.80 5000 52 78 m/z 78.05 19.35%

35 87 1____ _............. . li| mmmpmpmp " I" H1111' I > r> f t rr ■ | > < i"1' i" " i' H111' +TJT TTTTTTT miz-> 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 200 210 Abundance #66892: Benzaldehyde, 2-hydroxy-3-methoxy- .... ,—।—।——r—।—r—।—, — , 4—, — । । > । । 1$2 1120 11.40 11.60 11.80 m/z 52.00 14.11% 106 5000 53 81

92 122 i il 136 '"I" "I1' TTTTT TVTTTTTTTTTTTTTTTTTT ■' i''' ■ I ■''' i . । ... । । ■ TTT TTTrufr m/z—> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 11.20 11.40 11.60 11.80

LBA.D GCMS1126.M Tue Nov 27 12:44:12 2001 Page 1

NYC-WTC_000033713

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NYC-WTC_000033713Source: NYC Law Department, mirrored locally

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GCMS comments for sample AD28157, Nov 2001 · Box DEP Box 21

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Analytical commentary for sample AD28157 dated November 29, 2001, noting no unusual compounds but low recovery rates for LCS standards.

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GCMS comments for sample AD28149, Nov 2001 · Box DEP Box 21

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Analytical commentary for sample AD28149 dated November 29, 2001, noting no unusual compounds but low recovery rates for LCS standards.

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