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GCMS analysis results for sample AD27569, Dec 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of environmental sample AD27569 conducted on December 18, 2001.

NYC-WTC_000033521–000033534

Folder label: “GCMS X 11/15/01 A 12/13/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\l\DATA\DEC1301\27569.D Vial: 10 Acq On 13 Dec 2001 6:34 pm Operator: GALOS Sample : gems unknown 11/15 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 5.181 34 37 45 rVB 60793 116913 1.48% 0.286% 2 6.107 135 138 144 rBV 39168 88563 1.12% 0.217% 3 6.446 171 175 184 rBV 41196 96091 1.21% 0.235% 4 6.556 184 187 198 rW2 77912 202594 2.56% 0.495% 5 6.685 198 201 210 rW 38855 86123 1.09% 0.211%

6 6.804 210 214 225 rW 47055 116543 1.47% 0.285% 7 7.822 321 325 341 rBV 462087 963701 12.18% 2.356% 8 10.289 590 594 602 rBV 163830 304568 3.85% 0.745% 9 10.499 613 617 627 rBV 188260 342055 4.32% 0.836% 10 10.820 648 652 659 rBV 118374 228958 2.89% 0.560%

11 11.857 760 765 775 rBV 2897063 5976871 75.55% 14.612% 12 15.470 1153 1159 1177 rBV 4094795 7911334 100.00% 19.341% 13 20.742 1728 1734 1750 rBV 3859645 7643816 96.62% 18.687% 14 25.153 2208 2215 2226 rBV2 3365658 7151818 90.40% 17.484% 15 33.150 3081 3087 3100 rBV2 2414415 5288788 66.85% 12.930%

16 37.230 3524 3532 3555 rBV2 1643958 4385273 55.43% 10.721%

Sum of corrected areas: 40904009

27569.D NP112701.M Fri Dec 14 12:57:51 2001

NYC-WTC_000033527

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NYC-WTC_000033527Source: NYC Law Department, mirrored locally

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