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GCMS analysis results for sample AD27549, Dec 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of environmental sample AD27549 conducted on December 18, 2001.

NYC-WTC_000033490–000033504

Folder label: “GCMS X 11/15/01 A 12/13/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\l\DATA\DEC1301\27549.D Vial: 8 Acq On 13 Dec 2001 4:45 pm Operator: GALOS Sample : gems unknown 11/15 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 5.185 34 37 52 rVB 60234 162541 1.91% 0.375% 2 6.551 183 186 189 rBV 74526 136028 1.60% 0.314% 3 6.799 210 213 218 rBV 51636 103907 1.22% 0.240% 4 7.826 321 325 342 rVB 434472 967403 11.37% 2.234% 5 10.292 590 594 603 rVB 113234 216654 2.55% 0.500%

6 10.503 613 617 625 rBV 121743 230792 2.71% 0.533% 7 10.824 648 652 658 rBV 80043 158801 1.87% 0.367% 8 11.860 760 765 784 rVB 3182545 6564564 77.19% 15.157% 9 15.473 1153 1159 1176 rBV 4378729 8504717 100.00% 19.636% 10 20.746 1728 1734 1748 rBV 4098447 8163728 95.99% 18.849%

11 25.148 2208 2214 2226 rBV2 3621849 7696751 90.50% 17.771% 12 33.153 3080 3087 3112 rBV2 2621136 5800290 68.20% 13.392% 13 '37.234 3524 3532 3553 rBV2 1732871 4605435 54.15% 10.633%

Sum of corrected areas: 43311611

27549.D NP112701.M Fri Dec 14 12:56:36 2001

NYC-WTC_000033496

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NYC-WTC_000033496Source: NYC Law Department, mirrored locally

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