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GCMS analysis results for sample AD27548, Dec 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of environmental sample AD27548 conducted on December 18, 2001.

NYC-WTC_000033474–000033489

Folder label: “GCMS X 11/15/01 A 12/13/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\1\DATA\DEC13 01\27548.D Vial: 7 Acq On 13 Dec 2001 3:50 pm Operator: GALOS Sample : gems unknown 11/15 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 5.200 36 39 52 rVB 63075 144058 l. 74% 0.325% 2 6.117 135 139 146 rBV 37439 87161 1.05% 0.197% 3 6.456 172 176 184 rBV 48316 104651 1.26% 0.236% 4 6.566 184 188 198 rW2 95286 237471 2.87% 0.536% 5 6.694 198 202 211 rVB 43004 90305 1.09% 0.204%

6 6.804 211 214 226 rBV 62197 145597 1.76% 0.329% 7 7.832 322 326 343 rBV 239825 539533 6.51% 1.219% 8 10.298 590 595 603 rBV 135242 264909 3.20% 0.598% 9 10.500 612 617 628 rBV 163186 301143 3.63% 0.680% 10 10.830 648 653 660 rBV 114355 210324 2.54% 0.475%

11 11.866 760 766 783 rVB 3053520 6332111 76.42% 14.304% 12 15.470 1153 1159 1177 rBV 4220520 8286230 100.00% 18.718% 13 20.743 1728 1734 1752 rBV 3974180 8040105 97.03% 18.162% 14 25.154 2208 2215 2226 rBV2 3774765 7795553 94.08% 17.610% 15 33.150 3080 3087 3107 rBV2 2871061 6359923 76.75% 14.367%

16 37.231 3524 3532 3552 rBV 1976110 5329591 64.32% 12.039%

Sum of corrected areas: 44268665

27548 .D NP112701.M Fri Dec 14 12:55:57 2001

NYC-WTC_000033480

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NYC-WTC_000033480Source: NYC Law Department, mirrored locally

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