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GCMS analysis results for sample AD27544, Dec 2001

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Laboratory report documenting GCMS analysis of sample AD27544 for unknown compounds and surrogates on December 18, 2001.

NYC-WTC_000033417–000033432

Folder label: “GCMS X 11/15/01 A 12/13/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\l\DATA\DEC1301\27544.D Vial: 3 Acq On : 13 Dec 2001 12:12 pm Operator: GALOS Sample : gems unknown 11/15 Inst : GC/MS Ins Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 5.133 27 32 36 rBV 64643 115355 1.15% 0.213% 2 5.197 36 39 53 rVB 89947 200982 2.00% 0.372% 3 6.114 135 139 147 rBV 56368 127809 1.27% 0.236% 4 6.453 172 176 184 rBV 61122 132345 1.32% 0.245% 5 6.563 184 188 198 rW2 115197 289847 2.89% 0.536%

6 6.692 198 202 210 rVB 61090 125359 1.25% 0.232% 7 6.802 210 214 227 rBV 77719 193044 1.92% 0.357% 8 7.829 322 326 339 rBV 443509 927721 9.24% 1.716% 9 10.296 590 595 603 rVB 152350 293474 2.92% 0.543% 10 10.497 613 ' 617 628 rBV 176752 334196 3.33% 0.618%

11 10.828 648 653 658 rBV 113809 206815 2.06% 0.383% 12 11.864 760 766 779 rVB 3729288 7682552 76.51% 14.212% 13 15.468 1153 1159 1173 rBV 5007103 10041211 100.00% 18.576% 14 20.740 1728 1734 1746 rBV 4883429 9852847 98.12% 18.227% 15 25.151 2208 2215 2226 rBV2 4523164 9367366 93.29% 17.329%

16 33.157 3080 3088 3106 rBV2 3418119 7698184 76.67% 14.241% 17 37.237 3524 3533 3551 rBV2 2424581 6466312 64.40% 11.962%

Sum of corrected areas: 54055419

27544.D NP112701.M Fri Dec 14 12:53:42 2001

NYC-WTC_000033423

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NYC-WTC_000033423Source: NYC Law Department, mirrored locally

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