GCMS calibration data, Dec 2001

NYC 9/11 Public Portal Document

LSC Area Percent Report

• Data File : C:\HPCHEM\1\DATA\DEC210128171.D Vial: 37 Acq On : 22 Dec 2001 1:59 pm Operator: GALOS Sample : gems unknown 11/26 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 5.147 30 33 41 rVB 45938 79516 1.16% 0.219% 2 6:403 165 170 176 rBV 52186 100370 1.46% 0.276% 3 6.504 176 181 184 rBV 98941 179757 2.62% 0.494% - 4 6.633 192 195 202 rVB 40087 75945 1.11% 0.209% 5 6.743 204 207 217 rW 61578 129481 1.89% 0.356%

6 7.770 315 319 333 rBV 280720 578319 8.42% 1.590% 7 10.227 583 587 594 rVB 86272 142083 2.07% 0.391% 8 10.438 606 610 617 rBB 97008 169133 2.46% 0.465% 9 10.759 641 645 651 rBV 87726 152474 2.22% 0.419%, 10 11.786 751 757 770 rBV 2642054 5289136 77.01% 14.537%'

11 15.399 1144 1151 1167 rBV 3146455 6868137 100.00% 18.877% 12 20.672 1718 1726 1741 rBV 3165118 6727360 97.95% 18.490% 13 25.083 2199 2207 2217 rBV2 2995351 6503146 94.69% 17.874% 14 33.088 3073 3080 3090 rBV2 2338696 5396475 78.57% 14.832% 15 37.160 3515 3524 3534 rBV2 1486104 3991667 58.12% 10.971%

Sum of corrected areas: 36382999

28171.D NP112701.M Fri Dec 28 09:07:28 2001

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