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GCMS analysis results for sample AD28104, Jan 2002

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Laboratory report documenting GCMS analysis of sample AD28104 conducted on January 2, 2002.

NYC-WTC_000034615–000034630

Folder label: “GCMS X 11/23/01 A 12/21/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C : \HPCHEM\ 1 \DATA\DEC2101\28167.D Vial: 17 Acq On : 22 Dec 2001 9:25 am Operator: GALOS Sample : gems unknown 11/23 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 5.062 21 24 28 rBV 35257 61531 1.09% 0.200% 2 5.126 28 31 36 rVB 44280 77972 1.38% .253% 3 6.043 128 131 138 rBV 28360 56806 1.00% 0.184% 4 6.383 164 168 173 rBV 61627 113280 2.00% 0.367% 5 6.483 176 179 183 rBV 102387 200435 3.54% 0.650%

6 6.621 190 194 202 rBV 43252 87091 1.54% 0.282% 7 6.731 202 206 217 rBV 68854 140276 2.48% 0.455% 8 7.749 313 317 335 rBB 424763 915618 16.18% 2.969% 9 10.225 583 587 594 rVB 102250 172370 3.05% 0.559% 10 10.436 605 610 618 rBV 123003 202018 3.57% 0.655%

11 10.757 641 645 651 rBV 104581 188659 3.33% 0.612% 12 11.784 752 757 767 rBV 2214089 4396661 77.68% 14.259% 13 14.416 1040 1044 1049 rBB2 55554 106361 1.88% 0.345% 14 15.397 1144 1151 1164 rBV 2747919 5659631 100.00% 18.355% 15 20.670 1719 1726 1738 rBV 2638752 5486505 96.94% 17.793%

16 25.080 2200 2207 2217 rBV2 2462671 5328212 94.14% 17.280% 17 33.077 3072 3079 3091 rBV2 1905670 4411084 77.94% 14.305% 18 37.148 3515 3523 3538 rBV2 1210761 3230549 57.08% 10.477%

Sum of corrected areas: 30835059

28167.D NP112701.M Fri Dec 28 09:57:57 2001

NYC-WTC_000034621

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NYC-WTC_000034621Source: NYC Law Department, mirrored locally

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