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GCMS analysis results for sample AD27768, Jan 2002

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Laboratory report documenting GCMS analysis of sample AD27768 for unknown compounds and surrogates on January 3, 2002.

NYC-WTC_000033373–000033387

Folder label: “GCMS X 11/16/01 A 12/18 - 12/20/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\l\DATA\DEC1901\27768.D Vial: 11 Acq On : 20 Dec 2001 5:02 am Operator: GALOS Sample : gems unknown 11/16 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 5.242 41 44 53 rVB 62427 112718 1.30% 0.236% 2 6.489 173 180 185 rBV 401585 759530 8.76% 1.589% 3 6.590 185 191 195 rBV 708872 1389024 16.01% 2.907% 4 6.728 201 206 212 rVB 358538 679347 7.83% 1.422% 5 6.838 212 218 226 rBV 512833 997325 11.50% 2.087%

6 7.782 317 321 325 rBV 156528 281326 3.24% 0.589% 7 7.856 325 329 340 rW 556551 1125317 12.97% 2.355% 8 9.644 520 524 527 rBV 47435 96684 1.11% 0.202% 9 11.872 761 767 777 rVB 3149571 6661428 76.80% 13.941% 10 14.495 1047 1053 1057 rBV 45141 98719 1.14% 0.207%

11 15.485 1153 1161 1177 rBV 3275227 8673424 100.00% 18.151% 12 20.758 1727 1736 1751 rBV 3395633 8492638 97.92% 17.773% 13 25.178 2206 2218 2227 rBV2 3308096 7998036 92.21% 16.738% 14 25.306 2228 2232 2238 rVB 38071 89865 1.04% 0.188% 15 33.174 3082 3090 3102 rVB2 2664877 6332246 73.01% 13.252%

16 33.422 3114 3117 3122 rVB2 42923 87760 1.01% 0.184% 17 37.264 3528 3536 3546 rVB2 1413732 3909214 45.07% 8.181%

Sum of corrected areas: 47784601

27768 .D NP112701.M Thu Dec 20 11:46:28 2001

NYC-WTC_000033379

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NYC-WTC_000033379Source: NYC Law Department, mirrored locally

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