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GCMS analysis results for sample AD28166, Jan 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD28166 conducted on January 2, 2002.

NYC-WTC_000034669–000034685

Folder label: “GCMS X 11/23/01 A 12/21/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

‘ Data File : C:\HPCHEM\l\DATA\DEC2101\28165.D Vial: 15 Acq On : 22 Dec 2001 6:40 am Operator: GALOS Sample : gems unknown 11/23 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 5.156 31 34 42 rVB 44576 82467 1.18% 0.221% 2 6.403 165 170 176 rBV 81000 144005 2.06% 0.386% 3 6.504 176 181 185 rW 145188 278859 3.98% 0.748% 4 6.632 191 195 203 rVB 60382 114395 1.63% 0.307% 5 6.752 203 208 215 rBV 91363 184361 2.63% 0.495%

6 7.760 314 318 331 rBV 465588 952985 13.60% 2.557% 7 10.227 582 587 593 rBV 156119 256070 3.66% 0.687% 8 10.438 605 610 620 rVB 183386 317576 4.53% 0.852% 9 10.759 640 645 651 rBV 163382 284314 4.06% 0.763% 10 11.786 751 757 768 rVB 2648712 5340795 76.24% 14.328%

11 15.399 1143 1151 1163 rBV 3111194 7004793 100.00% 18.792% 12 20.672 1718 1726 1744 rBV 3065439 6762946 96.55% 18.143% 13 25.083 2199 2207 2218 rBV2 2939466 6425306 91.73% 17.237% 14 33.088 3072 3080 3097 rBV2 2216316 5182195 73.98% 13.903% 15 37.160 3515 3524 3540 rBV2 1444522 3944182 56.31% 10.581%

Sum of corrected areas: 37275249

28165.D NP112701.M Fri Dec 28 09:56:59 2001

NYC-WTC_000034675

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NYC-WTC_000034675Source: NYC Law Department, mirrored locally

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