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GCMS analysis results for sample AD28167, Jan 2002

Machine-extracted title · confidence 90%

Laboratory report documenting GCMS analysis of sample AD28167 conducted on January 2, 2002.

NYC-WTC_000034596–000034614

Folder label: “GCMS X 11/23/01 A 12/21/01

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NYC 9/11 Public Portal Document LSC Area Percent Report

'.Data-File : C:\HPCHEM\l\DATA\DEC2101\28168.D Vial: 18 •Acq On : 22 Dec 2001 10:19 am Operator: GALOS Sample : gems unknown 11/23 Inst : GC/MS Ins Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 5.148 30 33 43 rVB 53956 101805 1.51% 0.280% 2 6.395 165 169 176 rBV 71325 138999 2.06% 0.383% 3 6.505 176 181 185 rBV 133641 264255 3.92% 0.728% 4 6.634 191 195 202 rVB 57581 106182 1.57% 0.292% 5 6.744 202 207 216 rBV 86198 177066 2.63% 0.488%

6 7.762 314 318 332 rBV 498640 961631 14.26% 2.648% 7 10.219 582 586 592 rVB 157500 288993 4.29% 0.796% 8 10.430 605 609 617 rBV 198585 350819 5.20% 0.966% . 9 10.760 640 645 650 rBV 169426 312514 4.63% 0.861% 10 11.778 751 756 770 rVB 2449974 5211802 77.29% 14.353%

11 15.391 1143 1150 1168 rBV 2969856 6743181 100.00% 18.570% 12 20.673 1718 1726 1741 rBV 2912174 6599032 97.86% 18.173% 13 25.084 2198 2207 2216 rBV2 2793257 6310534 93.58% 17.378% 14 33.080 3072 3079 3092 rBV2 2218661 5033646 74.65% 13.862% 15 37.152 3515 3523 3535 rBV2 1344280 3712356 55.05% 10.223%

Sum of corrected areas: 36312815

28168.D NP112701.M Fri Dec 28 09:58:49 2001

NYC-WTC_000034602

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NYC-WTC_000034602Source: NYC Law Department, mirrored locally

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