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GCMS analysis results for sample AD27628, Jan 2002

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Laboratory report documenting GCMS analysis of sample AD27628 for unknown compounds and surrogates on January 3, 2002.

NYC-WTC_000033159–000033176

Folder label: “GCMS X 11/16/01 A 12/18 - 12/20/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

. Data File : C:\HPCHEM\1\DATA\DEC1901\27628.D Vial: 18 Acq On : 20 Dec 2001 1:24 pm Operator: GALOS Sample : gems unknown 11/16 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 4.997 14 17 23 rBV 273972 484605 7.95% 1.472% 2 5.143 30 33 50 rVB2 34041 131747 2.16% 0.400% 3 6.436 170 174 182 rBV 143498 298460 4.89% 0.907% 4 6.546 182 186 195 rW 223332 520856 8.54% 1.582% 5 6.666 195 199 208 rW 123756 259498 4.26% 0.788%

6 6.785 208 212 222 rVB 140923 290261 4.76% 0.882% 7 7.748 313 317 322 rBV 79490 168438 2.76% 0.512% 8 7.830 322 326 342 rVB 622071 1323684 21.71% 4.021% 9 11.865 761 766 780 rBV 2250074 4724044 77.47% 14.351% 10 15.487 1155 1161 1179 rBV 2842748 6097649 100.00% 18.524%

11 20.751 1729 1735 1759 rBV 2698319 5929656 97.24% 18.014% 12 25.162 2210 2216 2228 rBV2 2453127 5539065 90.84% 16.827% 13 33.167 3082 3089 3099 rBV2 1925850 4378807 71.81% 13.303% 14 35.689 3359 3364 3371 rBV4 36336 92433 1.52% 0.281% 15 37.248 3527 3534 3542 rBV2 981040 2677557 43.91% 8.134%

Sum of corrected areas: 32916760

27628.D NP112701.M Fri Dec 21 09:18:58 2001

NYC-WTC_000033165

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NYC-WTC_000033165Source: NYC Law Department, mirrored locally

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