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GCMS analysis results for sample AD28168, Jan 2002

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Laboratory report documenting GCMS analysis of sample AD28168 conducted on January 2, 2002.

NYC-WTC_000034579–000034595

Folder label: “GCMS X 11/23/01 A 12/21/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

‘Data File : C:\HPCHEM\l\DATA\DEC2101\28164.D Vial: 14 Acq'On : 22 Dec 2001 5:46 am Operator: GALOS Sample : gems unknown 11/23 Inst : GC/MS Ins Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 5.148 30 33 43 rVB 54279 99695 1.31% 0.241% 2 6.404 163 170 176 rBV 81927 153338 2.01% 0.371% 3 6.505 176 181 191 rW 156559 339078 4.46% 0.820% 4 6.633 191 195 203 rVB 63375 122847 1.61% 0.297% 5 6.743 203 207 218 rBV 98387 200995 2.64% 0.486%

6 7.761 314 318 331 rBV 755684 1493059 19.62% 3.611% 7 10.228 583 587 593 rVB 146472 245534 3.23% 0.594% 8 10.439 605 610 618 rBV 180724 306842 4.03% 0.742% 9 10.760 641 645 650 rBV 154370 270070 3.55% 0.653% 10 11.787 752 757 768 rVB 2936204 5826981 76.57% 14.093% 11 15.400 1144 1151 1167 rBV 3549230 7609978 100.00% 18.405% 12 20.672 1718 1726 1741 rBV 3405999 7452132 97.93% 18.024% 13 25.083 2199 2207 2218 rBV2 3276132 7097907 93.27% 17.167% 14 33.089 3073 3080 3092 rBV2 2522951 5767329 75.79% 13.949% 15 37.160 3515 3524 3538 rBV2 1627851 4360555 57.30% 10.546%

Sum of corrected areas: 41346340

28164.D NP112701.M Fri Dec 28 09:56:13 2001

NYC-WTC_000034585

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NYC-WTC_000034585Source: NYC Law Department, mirrored locally

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