GCMS analysis report, Jan 2002

NYC 9/11 Public Portal Document

LSC Area Percent Report

• Data File : C:\HPCHEM\1\DATA\DEC2101\28309.D Vial: 41 Acq On : 22 Dec 2001 5:37 pm Operator: GALOS Sample : gems unknown 11/26 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak .peak % of # min scan scan scan TY height area % max. total

1 5.150 31 34 39 rVB 43663 75882 1.11% 0.213% 2 6.406 166 171 176 rBV 49819 93983 1.37% 0.264% 3 6.507 176 182 192 rW 95039 203348 2.96% 0.570% 4 6.636 192 196 2 03 rW 39140 77265 1.13% 0.217% 5 6.746 204 208 217 rVB 57791 117217 1.71% 0.329%

6 7.764 315 319 334 rBV 321986 634504 9.25% 1.779% 7 10.221 583 587 595 rBV 101528 188219 2.74% 0.528% 8 10.432 606 610 617 rVB 125851 212889 3.10% 0.597% 9 10.753 641 645 651 rBV 99860 183886 2.68% 0.516% 10 11.780 752 757 765 rBV 2447628 5209433 75.90% 14.610%'

11 15.393 1144 1151 1168 rBV 2996008 6863203 100.00% 19.248% 12 20.666 1718 1726 1738 rBV 2893345 6618119 96.43% 18.560% 13 25.077 2199 2207 2218 rBV2 2834037 6367043 92.77% 17.856% 14 33.082 3073 3080 3094 rBV2 2265155 5081317 74.04% 14.250% 15 37.154 3516 3524 3541 rBV2 1419501 3731142 54.36% 10.464%

Sum of corrected areas: 35657450

28309.D NP112701.M Fri Dec 28 09:10:01 2001

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