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GCMS analysis results, sample AD27547, December 2001

Machine-extracted title · confidence 85%

Gas chromatography-mass spectrometry analysis of environmental sample AD27547 performed on 12/18/01, detecting unknown compounds with 2,4-DDD surrogate standard at 5.0 ug MDL.

NYC-WTC_000033458–000033473

Folder label: “GCMS X 11/15/01 A 12/13/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\1\DATA\DEC1301\27547.D Vial: 6 Acq On 13 Dec 2001 2:56 pm Operator: GALOS Sample : gems unknown 11/15 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 5.192 35 38 53 rVB 74669 170558 1.75% 0.334% 2 6.457 171 176 182 rBV 54411 111709 1.15% 0.219% 3 6.558 184 187 190 rBV 94447 170303 1.75% 0.333% 4 6.805 210 214 225 rBV 65132 153054 1.57% 0.300% 5 7.833 322 326 343 rVB 395565 895130 9.19% 1.752%

6 10.290 ■ 590 594 601 rBV 139182 273188 2.80% 0.535% 7 10.501 612 617 626 rBV 164166 308078 3.16% 0.603% 8 10.831 ' 64 3 653 657 rBV 111626 210340 2.16% 0.412% 9 11.867 760 766 778 rBV 3612109 7489179 76.85% 14.662% 10 15.471 1153 1159 1177 rBV 5004956 9744790 100.00% 19.078%

11 20.744 1728 1734 1750 rBV 4652397 9455192 97.03% 18.511% 12 25.155 2208 2215 2226 rBV2 4327352 9019633 92.56% 17.658% 13 33.151 3080 3087 3106 rBV2 3254788 7238982 74.29% 14.172% 14 37.241 3524 3533 3554 rBV2 2166415 5838963 59.92% 11.431%

Sum of corrected areas: 51079099

27547.D NP112701.M Fri Dec 14 12:55:15 2001

NYC-WTC_000033464

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NYC-WTC_000033464Source: NYC Law Department, mirrored locally

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