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GCMS analysis report, Jan 2002

Machine-extracted title · confidence 100%

Laboratory report detailing GCMS results for sample AD28172 analyzed on January 3, 2002.

NYC-WTC_000035381–000035395

Folder label: “GCMS X 11/26/01 A 12/22/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\1\DATA\DEC2101\28308.D Vial: 40 Acq On 22 Dec 2001 4:43 pm Operator: GALOS Sample : gems unknown 11/26 Inst : .GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height . area % max. total

1 6.402 165 170 175 rBV 50842 93998 1.34% 0.257% 2 6.503 175 181 184 rBV 94199 170851 2.43% 0.467% 3 6.631 192 195 203 rVB 39133 74514 1.06% 0.204% 4 6.741 203 207 218 rBV 58786 124418 1.77% 0.340% 5 7.768 315 319 330 rBV 273991 549333 7.83% 1.502%

6 10.226 583 587 593 rBB 81500 137030 1.95% 0.375% 7 10.437 605 610 617 rBB 92833 157569 2.25% 0.431% 8 10.758 641 645 650 rBV 82630 144880 2.06% 0.396% 9 11.785 752 757 767 rBV 2665977 5410147 77.10% 14.796%, 10 15.398 1144 1151 1167 rBV 3254658 7017150 100.00% 19.190%

11 20.670 1719 1726 1739 rBV 3198701 6766525 96.43% 18.505% 12 25.081 2200 2207 2218 rBV2 2984456 6498310 92.61% 17.771% 13 33.087 3073 3080 3095 rBV2 2300092 5351929 76.27% 14.636% 14 37.158 3516 3524 3538 rBV2 1490955 4069265 57.99% 11.129%

Sum of corrected areas: 36565919

28308.D NP112701.M Fri Dec 28 09:09:24 2001

NYC-WTC_000035386

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NYC-WTC_000035386Source: NYC Law Department, mirrored locally

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