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GCMS analysis results for sample AD27957, Jan 2002

Machine-extracted title · confidence 95%

Laboratory report detailing GCMS analysis of sample AD27957 conducted on January 2, 2002.

NYC-WTC_000034138–000034153

Folder label: “GCMS X 11/20/01 A 12/20/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\l\DATA\DEC1901\27957.D Vial: 13 Acq On : 21 Dec 2001 3:06 am Operator: GALOS Sample : gems unknown 11/20 Inst :•GC/MS Ins Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 6.465 172 177 183 rBV 130276 251050 2.20% 0.425% 2 6.576 183 189 198 rW 231264 497825 4.36% 0.843% 3 6.704 198 203 210 rW 113177 202582 1.77% 0.343% 4 6.814 210 215 225 rVB 149198 297433 2.60% 0.503% 5 7.832 322 326 339 rBV 517707 1056382 9.24% 1.788%

6 11.858 759 765 779 rBV 4187008 8678116 75.92% 14.689% 7 15.471 1151 1159 1175 rBV 4554695 11430427 100.00% 19.348% 8 20.752 1726 1735 1753 rBV 4384897 11089611 97.02% 18.771% 9 25.163 2206 2216 2226 rBV2 4568611 10580055 92.56% 17.908%' 10 25.292 2226 2230 2241 rVB 50975 129159 1.13% 0.219%

11 29.556 2689 2695 2701 rVB 123485 237712 2.08% 0.402% 12 31.683 2921 2927 2933 rBV2 97845 209872 1.84% 0.355% 13 31.775 2933 2937 2947 rVB 61446 132556 1.16% 0.224% 14 33.169 3080 3089 3101 rBV2 3631894 8683786 75.97% 14.699% 15 37.259 3525 3535 3548 rBV2 1912710 5602207 49.01% 9.483%

Sum of' corrected areas: 59078773

27957.D NP112701.M Fri Dec 21 10:07:10 2001

NYC-WTC_000034144

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NYC-WTC_000034144Source: NYC Law Department, mirrored locally

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