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GCMS analysis results for sample AD27545, Dec 2001

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Laboratory report documenting GCMS analysis of sample AD27545 for unknown compounds and surrogates on December 18, 2001.

NYC-WTC_000033433–000033447

Folder label: “GCMS X 11/15/01 A 12/13/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File-: C:\HPCHEM\1\DATA\DEC1301\27545.D Vial: 4 Acq On 13 Dec 2001 1:07 pm Operator: GALOS Sample : gems unknown 11/15 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge 100 prefer < Baseline drop else tangent Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. .total

1 5.194 35 38 53 rVB 88324 188577 1.78% 0.341% 2 6.120 136 139 144 rBV 56992 111183 1.05% 0.201% 3 6.459 172 176 181 rBV 72083 135095 1.27% 0.244% 4 6.560 184 187 198 rW2 128975 325629 3.07% 0.588% 5 6.698 198 202 210 rW 63963 133088 1.25% 0.240%

6 6.808 210 214 226 rW 85486 191991 1.81% 0.347% 7 7.835 322 326 340 rVB 428662 952826 8.97% 1.722% 8 10.292 590 594 603 rVB 119064 213387 2.01% 0.386% 9 10.503 613 617 628 rVB 131670 241293 2.27% 0.436% 10 10.824 648 652 657 rBV 85814 158273 1.49% 0.286%

11 11.861 760 765 779 rBV 4106891 8190617 77.15% 14.801% 12 15.474 1153 1159 1176 rBV 5389814 10616983 100.00% 19.185% 13 20.746 1727 1734 1749 rBV 5021047 10215991 96.22% 18.461% 14 25.157 2208 2215 2226 rBV2 4610237 9763928 91.97% 17.644% 15 33.153 3080 3087 3101 rBV2 3448123 7652351 72.08% 13.828%

16 37.234 3523 3532 3556 rBV2 2312593 6247924 58.85% 11.290%

Sum of corrected areas: 55339136

27545.D NP112701.M Fri Dec 14 12:54:22 2001

NYC-WTC_000033439

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NYC-WTC_000033439Source: NYC Law Department, mirrored locally

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