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GCMS analysis results for sample AD27638, Jan 2002

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of sample AD27638 for unknown compounds and surrogates on January 3, 2002.

NYC-WTC_000033206–000033220

Folder label: “GCMS X 11/16/01 A 12/18 - 12/20/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\1\DATA\DEC1901\27638.D Vial: 21 Acq On : 20 Dec 2001 4:09 pm Operator: GALOS Sample : gems unknown 11/16 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 6.476 170 178 183 rBV 145882 289356 3.93% 0.760% 2 6.577 183 189 193 rBV 271821 529219 7.19% 1.391% 3 6.706 199 203 210 rVB 133577 236346 3.21% 0.621% 4 6.816 210 215 223 rBV 183275 353288 4.80% 0.928% 5 7.769 315 319 323 rBV 92617 167701 2.28% 0.441%

6 7.843 323 327 342 rVB 546290 1097735 14.91% 2.885% 7 11.859 760 765 777 rVB 2735527 5717330 77.64% 15.025% 8 15.472 1152 1159 1176 rBV 3121696 7364020 100.00% 19.352% 9 20.745 1727 1734 1761 rBV 3027298 7162231 97.26% 18.822% 10 25.165 2207 2216 2227 rBV2 3053104 6773424 91.98% 17.800%

11 33.161 3079 3088 3102 rBV2 2210550 5180872 70.35% 13.615% 12 37.251 3526 3534 3544 rVB2 1189893 3181511 43.20% 8.361%

Sum of corrected areas: 38053033

27638 .D NP112701.M Fri Dec 21 09:20:55 2001

NYC-WTC_000033212

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NYC-WTC_000033212Source: NYC Law Department, mirrored locally

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