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GCMS analysis results for sample AD27632, Jan 2002

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of sample AD27632 for unknown compounds and surrogates on January 3, 2002.

NYC-WTC_000033191–000033205

Folder label: “GCMS X 11/16/01 A 12/18 - 12/20/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\l\DATA\DEC1901\27632.D Vial: 20 Acq On : 20 Dec 2001 3:14 pm Operator: GALOS Sample : gems unknown 11/16 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak . peak peak % of # min scan scan scan TY height area % max. total

1 6.476 172 178 183 rBV 143641 273032 3.90% 0.743% 2 6.577 183 189 193 rBV 277082 533984 7.62% 1.453% 3 6.705 199 203 211 rVB 128774 236708 3.38% 0.644% 4 6.815 211 215 223 rBV 173596 347327 4.96% 0.945% 5 7.769 315 319 323 rBV 144375 268893 3.84% 0.732%

6 7.842 323 327 341 rVB 405225 806429 11.51% . 2.195% 7 11.868 760 766 779 rBV 2531667 5403501 77.10% 14.708% 8 15.472 1152 1159 1177 rBV 2816484 7008847 100.00% 19.077% 9 20.754 1727 1735 1748 rBV 2896253 6845700 97.67% 18.633% 10 25.164 2207 2216 2226 rBV2 2996693 6539396 93.30% 17.799%

11 33.170 3080 3089 3098 rBV2 2327217 5207512 74.30% 14.174% 12 37.251 3526 3534 3545 rBV2 1216141 3268023 46.63% 8.895%

Sum of corrected areas: 36739352

27632.D NP112701.M Fri Dec 21 09:20:18 2001

NYC-WTC_000033197

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NYC-WTC_000033197Source: NYC Law Department, mirrored locally

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