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GCMS analysis results for sample AD27631, Jan 2002

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of sample AD27631 for unknown compounds and surrogates on January 3, 2002.

NYC-WTC_000033177–000033190

Folder label: “GCMS X 11/16/01 A 12/18 - 12/20/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\1\DATA\DEC1901\27631.D Vial: 19 Acq On : 20 Dec 2001 2:19 pm Operator: GALOS Sample : gems unknown 11/16 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 5.221 38 41 47 rVB2 37675 70258 1.00% 0.200% 2 6.477 170 178 183 rBV 170843 332551 4.74% 0.945% 3 6.578 . 183 189 193 rBV 348181 694470 9.89% 1.973% 4 6.706 199 203 210 rBV 154508 283279 4.04% 0.805% 5 6.816 210 215 224 rVB 225316 426332 6.07% 1.211%

6 7.779 315 320 324 rBV 36613 72712 1.04% 0.207% 7 7.853 324 328 338 rW 82342 193409 2.76% 0.549% 8 11.869 760 766 776 rVB 2543764 5374706 76.57% 15.268% 9 15.482 1152 1160 1177 rBV 2942508 7019351 100.00% 19.939% 10 20.755 1727 1735 1749 rBV 2974600 6761147 96.32% 19.206%

11 25.166 2208 2216 2227 rBV2 2900264 6350733 90.47% 18.040% 12 33.171 3082 3089 3100 rVB2 2079816 4774206 68.01% 13.562% 13 37.252 3526 3534 3542 rBV2 1061089 2850414 40.61% 8.097%

Sum of corrected areas: 35203568

27631.D NP112701.M Fri Dec 21 09:19:44 2001

NYC-WTC_000033183

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NYC-WTC_000033183Source: NYC Law Department, mirrored locally

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