GCMS results log, sample AD26984, Dec 11 2001

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Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC0601\26984.D Vial: 16 Acq On 6 Dec 2001 11:49 pm Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Cyclohexane, methyl- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

5.04 0.52 ng/uL .186173 1,4-Dichlorobenzene-d4 11.89

Hit# Of 5 Tentati ID MW MolForm CAS# Qual

l Cyclohexane, met hyl- 98 C7H14 000108-87-2 90 2 Cyclohexane, met hyl- 98 C7H14 000108-87-2 72 3 2-Pentene, 3,4-dimethyl-, (E) - 98 C7H14 004914-92-5 53 4 2-Pentene, 4,4-dimethyl-, (E) -________ 98 C7H14 000690-08-4 53 ’Abundance / Scan 22 (5.044 min): 26984.D (-) m/ z 83.05 100.00% / 55 83

5000 41 98 69 i •1111 । n . . | > i | ■ f < ■ | 4.90 5.00 5.10 5.20 5.30 5.40 5.50

m/z-> 5 TTTTTTTTTTTTTTTTTTTTT’TTTT Hp 1 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 ..... ........ I m/ Z 55.10 93.37% Abundance #1326: Cyclohexane, methyl- 83 55

5000- 98 TrArfr 42 4.90 5.00 5.10 5.20 5.30 5.40 5.50 27 69 m/ Z 41.00 47.29% I

M ।.i<*। | i। | |.i.i| " i" ■11 TTUTTTTr TT rrrrp-m J m/z--> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #63234: Cyclohexane, methyl- 55 83 i1 ■ ■ ■ r ''' i'''' i''' ■ i'''' I 4.90 5.00 5.10 5.20 5.30 5.40 5.50 5000 - m/z 98.05 40.36% 42 98 69 27 ............................... ■........................................................................ _....................................................... _

| r I I <|>I II | . i ti | . i t i | i i . . [ . i « i | TTTTICTCTTETTTIUTTUTTTTT’TTTTTTTTT 'm/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #1362: 2-Pentene, 3,4-dimethyl-, (E)- I • ‘ • i 55. 83 4.90 5.00 5.10 5.20 5.30 5.40 5.50 m/ Z: 42.05 32.95%

AA 5000 27 98 15 69

m/z-> 5 TTTTTTTTTTTTTTTTTTTTT ----?—5IL 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 । .......TI I" 1 'T MAA 4.90 5.00 5.10 5.20 5.30 5.40 5.50 I' ’1' I

26984.D NP112701.M Tue Dec 11 14:50:05 2001 Page 1

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