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GCMS comments for sample AD26475 showing no non-target compounds

Machine-extracted title · confidence 100%

Analysis report dated December 16, 2001, stating that mass spectrometry of sample AD26475 revealed no non-target compounds.

NYC-WTC_000031685–000031706

Folder label: “GCMS X 11/6/01 A 12/7/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

’ Data File C:\HPCHEM\1\DATA\DEC0701\26475.D Vial: 5 Acq On 7 Dec 2001 9:45 pm Operator: GALOS Sample gc/ms unknown 11/6 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 4.985 12 16 23 rBV 215400 456682 6.49% 1.000% 2 5.077 23 26 30 rW 215256 417216 5.93% 0.914% 3 5.141 30 33 56 rVB 345606 1242155 17.65% 2.721% 4 5.637 83 87 96 rVB3 44649 133131 1.89% 0.292% 5 6.086 132 136 154 rBV 181617 615331 8.74% 1.348%

6 6.444 171 175 182 rBV 71993 187057 2.66% 0.410% 7 6.554 183 187 197 rW 70913 197213 2.80% 0.432% 8 6.673 197 200 210 rW2 72879 235131 3.34% 0.515% 9 6.792 210 213 220 rVB2 45560 102676 1.46% 0.225%. 10 7.159 247 253 268 rBV 1748880 3427834 48.70% 7.507%

11 7.828 322 326 343 rVB 925893 2113189 30.02% 4.628% 12 9.341 486 491 504 rBV 48619 124989 1.78% 0.274% 13 10.313 592 597 607 rBV 360015 822222 11.68% 1.801% 14 10.515 615 619 627 rBV 176473 396501 5.63% 0.868% 15 11.872 762 767 779 rBV 2578531 5614082 79.76% 12.296%

16 15.494 1156 1162 1175 rBV 3390599 7029157 99.86% 15.395% 17 20.767 1730 1737 1753 rBV 3284560 7038951 100.00% 15.416% 18 25.178 2211 2218 2230 rBV2 2907931 6538698 92.89% 14.321% 19 25.316 2230 2233 2245 rVB 29517 83905 1.19% 0.184% 20 33.183 3084 3091 3111 rBV2 2091949 4950688 70.33% 10.843%

21 37.264 3528 3536 3559 rBV2 1432008 3932084 55.86% 8.612%

Sum of corrected areas: 45658892

26475.D NP112701.M Thu Dec 13 11:19:18 2001

NYC-WTC_000031691

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NYC-WTC_000031691Source: NYC Law Department, mirrored locally

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