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GCMS analysis sample AD26537, non-target compounds, Dec 2001

Machine-extracted title · confidence 95%

Mass spectrometry analysis of sample AD26537 found no non-target compounds present, Dec 16, 2001.

NYC-WTC_000031847–000031868

Folder label: “GCMS X 11/6/01 A 12/7/01

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NYC 9/11 Public Portal Document LSC Area Percent Report

• Data File C:\HPCHEM\1\DATA\DEC0 7 01\26537.D Vial: 4 Acq On 7 Dec 2001 8:51 pm Operator: GALOS Sample gc/ms unknown 11/6 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 4.980 12 15 21 rW 306747 575656 8.62% 1.232% 2 5.063 21 24 28 rW 171990 420971 6.30% 0.901% 3 5.136 28 32 56 rVB2 281277 1451537 21.73% 3.106% 4 5.622 81 85 105 rVB2 47420 259560 3.88% 0.555% 5 6.081 131 135 153 rBV 140249 631374 9.45% 1.351%

6 6.438 170 174 180 rBV 72660 195450 2.93% 0.418% 7 6.549 182 186 196 rW 76511 230713 3.45% 0.494% 8 6.668 196 199 209 rW 69172 240899 3.61% 0.516% 9 6.787 209 212 217 rVB3 43905 100992 1.51% 0.216% 10 7.172 247 254 267 rW 2966792 6359404 95.18% 13.609%

11 7.310° 267 269 280 rVB 25913 67814 1.01% 0.145% 12 7.823 319 325 344 rBV 729388 1890046 28.29% 4.045% 13 9.355 488 492 499 rBV 59950 147667 2.21% 0.316% 14 10.317 589 597 607 rBV 409268 973118 14.56% 2.082% 15 10.519 615 619 629 rBV 234023 515831 7.72% 1.104%

16 11.876 762 767 778 rW 2533833 5339949 79.92% 11.427% 17 15.489 1155 1161 1180 rBV 3322940 6681270 100.00% 14.298% 18 20.762 1730 1736 1754 rBV 3230194 6616496 99.03% 14.159% 19 23.531 2034 2038 2043 rBV 45100 86299 1.29% 0.185% 20 25.173 2211 2217 2229 rBV2 2776315 5994395 89.72% 12.828%

21 25.310^2229 2232 2241 rVB2 23983 70044 1.05% 0.150% 22 33.178 3084 3090 3108 rBV2 1968430 4437595 66.42% 9.496% 23 37.268 3529 3536 3553 rBV 1260916 3442328 51.52% 7.367%

Sum of corrected areas: 46729408

26537.D NP112701.M Thu Dec 13 11:26:59 2001

NYC-WTC_000031853

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NYC-WTC_000031853Source: NYC Law Department, mirrored locally

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