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GCMS comments for sample AD26478 showing no non-target compounds

Machine-extracted title · confidence 100%

Analysis report dated December 16, 2001, stating that mass spectrometry of sample AD26478 revealed no non-target compounds.

NYC-WTC_000031739–000031761

Folder label: “GCMS X 11/6/01 A 12/7/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File C:\HPCHEM\1\DATA\DEC0 701\26478.D Vial: 3 Acq On 7 Dec 2001 7:56 pm Operator: GALOS Sample gc/ms unknown 11/6 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\MBTHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 4.985 8 16 23 rBV 213416 476967 6.58% 0.996% 2 5.068 23 25 29 rW 161029 356150 4.91% 0.744% 3 5.141 29 33 59 rVB2 268856 1259530 17.37% 2.630% 4 5.627 83 86 107 rVB2 44607 212237 2.93% 0.443% 5 6.086 132 136 153 rBV 142782 612352 8.45% 1.278%

6 6.434 171 174 183 rBV 51239 162868 2.25% 0.340% 7 6.544 183 186 194 rW 58541 163192 2.25% 0.341% 8 6.673 197 200 202 rW2 59644 114833 1.58% 0.240% 9 6.709 202 204 210 rW 68426 158466 2.19% 0.331% 10 6.792 210 213 222 rVB 41357 101437 1.40% 0.212%

11 7.159 247 253 274 rVB 1788440 3660752 50.49% 7.643% 12 7.507 286 291 302 rBV 57649 122112 1.68% 0.255% 13 7.828 322 326 343 rBV 1012076 2353227 32.46% 4.913% 14 9.341 487 491 501 rBV 52083 126481 1.74% 0.264% 15 10.313 592 597 608 rBV 312554 717786 9.90% 1.499%

16 10.524 614 620 629 rBV 169907 367178 5.06% 0.767% 17 11.881 762 768 786 rBV 2726392 5839743 80.55% 12.192% 18 15.494 1156 1162 1180 rBV 3557419 7236019 99.81% 15.107% 19 20.767 1731 1737 1760 rBV 3463749 7249897 100.00% 15.136% 20 25.178 2211 2218 2229 rBV2 3140856 6754082 93.16% 14.101%

21 25.315 2230 2233 2244 rVB 28551 83543 1.15% 0.174% 22 33.183 3084 3091 3110 rBV 2395145 5378787 74.19% 11.230% 23 37.273 3529 3537 3559 rBV 1613822 4390275 60.56% 9.166%

Sum of corrected areas: 47897914

26478.D NP112701.M Thu Dec 13 11:21:56 2001

NYC-WTC_000031745

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NYC-WTC_000031745Source: NYC Law Department, mirrored locally

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