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GCMS Analysis Report for Sample AD26388, Dec 2001

Machine-extracted title · confidence 100%

Report documenting GCMS analysis of sample AD26388 with a note regarding unknown compounds.

NYC-WTC_000031452–000031472

Folder label: “GCMS X 11/5/01 A 12/1/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report Data File C:\HPCHEM\1\DATA\NOV3001\26388.D Vial: 14 Acq On 1 Dec 2001 12:02 am Operator: GALOS Sample gc/ms unknown 11/3 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Signal : TIC peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total 1 5.020 9 19 27 rBV 125680 591056 5.24% 0.801% 2 5.121 27 30 34 rW 484192 865260 7.67% 1.172% 3 5.185 34 37 55 rVB 732758 1753565 15.55% 2.375% 4 5.607 80 83 87 rW 68585 141844 1.26% 0.192% 5 5.671 87 90 103 rVB 113592 270347 2.40% 0.366% 6 6.120 135 139 156 rBV 413000 1027333 9.11% 1.391% 7 6.469 173 177 182 rBV 129045 256746 2.28% 0.348% 8 6.579 186 189 199 rVB 136598 304613 2.70% 0.413% 9 6.707 199 203 212 rBV 150300 370594 3.29% 0.502% 10 6.826 212 216 220 rBV 91688 175190 1.55% 0.237% 11 7.193 248 256 274 rVB 3008000 8078196 71.64% 10.941% 12 7.853 324 328 345 rBV 1117721 2350041 20.84% 3.183% 13 9.'357 488 492 505 rBV 125624 281259 2.49% 0.381% 14 10.329 593 598 607 rBV 940142 1975687 17.52% 2.676% 15 10.531 615 620 631 rBV 464985 947159 8.40% 1.283% 16 11.750 749 753 761 rBV2 114263 251345 2.23% 0.340% 17 11.888 763 768 782 rVB 4262671 8792768 77.98% 11.909% 18 15.501 1156 1162 1181 rBV 5442676 11275706 100.00% 15.272% 19 20.783 1731 1738 1756 rBV 5011837 10849790 96.22% 14.695% 20 25.194 2212 2219 2230 rBV2 4424170 9900458 87.80% 13.409% 21 33.190 3084 3091 3107 rBV2 3439298 7434469 65.93% 10.069% 22 37.280 3529 3537 3548 rBV2 2183682 5938537 52.67% 8.043%

Sum of corrected areas: 73831963 26388.D NP112701.M Tue Dec 04 10:40:16 2001

NYC-WTC_000031456

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NYC-WTC_000031456Source: NYC Law Department, mirrored locally

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