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GCMS results log, sample AD27009, Dec 11 2001

Machine-extracted title · confidence 100%

Laboratory report for GCMS analysis of sample AD27009 completed on December 11, 2001.

NYC-WTC_000032534–000032552

Folder label: “GCMS X 11/8/01 A 12/7/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

‘ Data File C:\HPCHEM\l\DATA\DEC0601\27009.D Vial: 28 Acq On 7 Dec 2001 11:38 am Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 5.052 17 23 27 rBV 122523 227146 1.77% 0.305% 2 6.592 187 191 201 rW 85674 187507 1.46% 0.251% 3 7.858 325 329 347 rVB 823116 1758532 13.68% 2.357% 4 10.324 594 598 606 rVB 66422 129658 1.01% 0.174% 5 10.526 614 620 629 rBV 65361 133336 1.04% 0.179%

6 11.893 763 769 780 rBV 4916146 10174139 79.15% 13.639% 7 15.496 1156 1162 1179 rBV 5875006 12854050 100.00% 17.232% 8 20.778 1731 1738 1755 rBV 5909769 12558666 97.70% 16.836% 9 25.189 2212 2219 2230 rBV2 5344975 11655117 90.67% 15.624% 10 29.591 2693 2699 2707 rBV 913171 1896884 14.76% 2.543%

11 29.701 2707 2711 2719 rW 151008 323601 2.52% 0.434% 12 30.774 2823 2828 2839 rBV 207411 449521 3.50% 0.603% 13 31.709 2925 2930 2936 rBV 573672 1336175 10.39% 1.791% 14 31.801 2936 2940 2951 rVB 417868 1012677 7.88% 1.358% 15 32.791 3042 3048 3061 rBV 340468 907033 7.06% 1.216%

16 33.195 3085 3092 3106 rBV2 3810837 8876435 69.06% 11.899% 17 33.745 3146 3152 3169 rBV 343239 1016132 7.91% 1.362% 18 34.671 3247 3253 3275 rBV 190723 702774 5.47% 0.942% 19 35.551 3343 3349 3363 rBV 120567 480707 3.74% 0.644% 20 36.404 3437 3442 3446 rBV4 49123 146512 1.14% 0.196%

21 37.284 3529 3538 3566 rBV2 2734060 7768863 60.44% 10.415%

Sum of corrected areas: 74595465

27009.D NP112701.M Tue Dec 11 14:59:13 2001

NYC-WTC_000032539

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NYC-WTC_000032539Source: NYC Law Department, mirrored locally

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