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GCMS results log, sample AD26833, Dec 11 2001

Machine-extracted title · confidence 100%

Laboratory report for GCMS analysis of sample AD26833 completed on December 11, 2001, showing surrogate recovery data.

NYC-WTC_000032286–000032307

Folder label: “GCMS X 11/8/01 A 12/7/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

’ Data File C:\HPCHEM\1\DATA\DEC0 6 01\26833.D Vial: 33 Acq On 7 Dec 2001 4:14 pm Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 5.036 15 21 31 rBV 96270 179649 1.90% 0.308% 2 6.585 186 190 194 rBV 53728 102332 1.08% 0.176% 3 7.851 324 328 344 rVB 468425 993698 10.54% 1.705% 4 11.886 763 768 . 785 rBV 3733481 7529759 79.83% 12.922% 5 15.499 1156 1162 1179 rBV 4538483 9432304 100.00% 16.187%

6 20.772 1731 1737 1756 rBV 4416544 9319797 98.81% 15.993% 7 25.182 2211 2218 2230 rBV2 4010084 8683120 92.06% 14.901% 8 25.320 2230 2233 2243 rVB 37300 95126 1.01% 0.163% 9 29.584 2693 2698 2706 rBV 992632 1980118 20.99% 3.398% 10 29.703 2706 2711 2720 rW 168273 394507 4.18% 0.677%

11 29.832 2720 2725 2737 rVB 73335 194492 2.06% 0.334% 12 30.776 2822 2828 2844 rBV 233291 524270 5.56% 0.900% 13 31.711 2924 2930 2936 rBV 578797 1288368 13.66% 2.211% 14 31.803 2936 2940 2951 rW 505920 1200767 12.73% 2.061% 15 32.794 3042 3048 3067 rBV 400170 1033681 10.96% 1.774%

16 33.188 3084 3091 3111 rBV2 2971145 6648811 70.49% 11.410% 17 33.747 3146 3152 3182 rBV 412247 1207877 12.81% 2.073% 18 34.664 3244 3252 3270 rBV 235481 809733 8.58% 1.390% 19 35.545 3342 3348 3364 rBV 148998 609193 6.46% 1.045% 20 36.407 3436 3442 3452 rBV3 62814 263538 2.79% 0.452%

21 37.278 3529 3537 3555 rBV 2066127 5781308 61.29% 9.921%

Sum of corrected areas: 58272448

26833.D NP112701.M Tue Dec 11 14:46:23 2001

NYC-WTC_000032292

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NYC-WTC_000032292Source: NYC Law Department, mirrored locally

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