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GCMS comments for sample AD26536 detecting 1,1,2,2-Tetrachloroethane

Machine-extracted title · confidence 100%

Analysis report dated December 16, 2001, identifying 1,1,2,2-Tetrachloroethane at 3.2 ug/L in sample AD26536.

NYC-WTC_000031831–000031846

Folder label: “GCMS X 11/6/01 A 12/7/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

- Data File C:\HPCHEM\1\DATA\DEC0 701\26536.D Vial: 11 Acq On 8 Dec 2001 3:14 am Operator: GALOS Sample gc/ms unknown 11/6 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge 100 prefer Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 5.040 18 22 35 rBV 688390 1689280 29.04% 4.748% 2 6.113 131 139 145 rBV4 16152 66704 1.15% 0.187% 3 6.471 174 178 186 rBV6 26647 97341 1.67% 0.274% 4 6.581 186 190 199 rBV 29396 70377 1.21% 0.198% 5 6.700 • 199 203 206 rBV 37710 97384 1.67% 0.274%

6 6.819 212 216 225 rVB2 28691 74374 1.28% 0.209% 7 7.186 251 256 274 rVB 1183203 2273807 39.09% 6.391% 8 7.855 325 329 349 rBV 669212 1699400 29.22% 4.777% 9 9.369 490 494 498 rBV 48026 87382 1.50% 0.246% 10 9.616 516 521 531 rVB 220352 766769 13.18% 2.155%'

11 10.322 593 598 606 rVB 35671 80253 1.38% 0.226% 12 10.533 615 621 629 rBV2 34343 80620 1.39% 0.227% 13 11.881 762 768 780 rBV 2138430 4745397 81.59% 13.339% 14 15.485 1156 1161 1181 rBV 2772001 5816496 100.00% 16.349% 15 17.649 1392 1397 1402 rBV 80751 147201 2.53% 0.414%

16 20.464 1699 1704 1708 rVB 56232 97797 1.68% 0.275% 17 20.758 1730 1736 1755 rBV 2816618 5791033 99.56% 16.278% 18 25.169 2208 2217 2229 rBV2 2366752 5217834 89.71% 14.666% 19 25.315 2229 2233 2242 rVB3 18047 64594 1.11% 0.182% 20 33.174 3084 3090 3111 rBV2 1715336 3929675 67.56% 11.046%

21 37.264 3529 3536 3550 rBV2 964813 2682869 46.13% 7.541%

Sum of corrected areas: 35576587

26536.D NP112701.M Thu Dec 13 11:25:44 2001

NYC-WTC_000031837

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NYC-WTC_000031837Source: NYC Law Department, mirrored locally

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