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GCMS comments for sample AD26476 showing no non-target compounds

Machine-extracted title · confidence 100%

Analysis report dated December 16, 2001, stating that mass spectrometry of sample AD26476 revealed no non-target compounds.

NYC-WTC_000031707–000031728

Folder label: “GCMS X 11/6/01 A 12/7/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

• Data File C:\HPCHEM\l\DATA\DEC0701\26476.D Vial: 6 Acq On 7 Dec 2001 10:40 pm Operator: GALOS Sample gc/ms unknown 11/6 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 5.005 12 18 24 rBV 224378 645467 ; 7.25% 1.171% 2 5.096 24 28 32 rW 328773 648558 7.28% 1.177% 3 5.160 32 35 56 rVB 505923 1382451 15.52% 2.509% 4 5.646 84 88 97 rVB 73126 168765 1.90% 0.306% 5 6.096 133 137 154 rBV 291463 793393 8.91% 1.440%

6 6.453 171 176 184 rBV 127902 309703 3.48% 0.562% 7 6.554 184 187 198 rVB 124235 280122 3.15% 0.508% 8 6.683 198 201 211 rBV 144512 372957 4.19% 0.677% 9 6.802 211 214 219 rBV 90779 178204 2.00% 0.323% 10 7.169 247 254 268 rBV 2102806 4224032 47.43% 7.665%

11 7.829 322 326 344 rVB 1113712 2314933 25.99% 4.201% 12 9.342 486 491 495 rBV 45175 94669 1.06% 0.172% 13 10.305 591 596 607 rBV 576636 1243256 13.96% 2.256% 14 10.516 614 619 628 rBV 328156 673359 7.56% 1.222% 15 11.873 762 767 777 rBV 3389032 7162271 80.43% 12.997%

16 14.505 1050 1054 1059 rBV 53783 96983 1.09% 0.176% 17 15.486 1155 1161 1180 rBV 4222045 8905481 100.00% 16.160% 18 20.768 1730 1737 1761 rBV 4070080 8725452 97.98% 15.833% 19 25.179 2209 2218 2229 rBV2 3442809 7779685 87.36% 14.117% 20 33.175 3084 3090 3105 rBV2 2252753 5177721 58.14% 9.395%

21 37.265 3529 3536 3553 rBV2 1420450 3931343 44.15% 7.134%

Sum of corrected areas: 55108805

26476.D NP112701.M Thu Dec 13 11:20:28 2001

NYC-WTC_000031713

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NYC-WTC_000031713Source: NYC Law Department, mirrored locally

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