Calibration data for GC/MS analysis using Method 508 and TCLP procedures dated November 30, 2001.
NYC-WTC_000030923–000030932Folder label: “GCMS SCAN X 11/2/01 AN 11/30/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File : C: \HPCHEM\ 1 \DATA\NOV3 001 \LBD. D Vial: 51 Acq On : 30 Nov 2001 3:40 pm Operator: 209 GALOS Sample : lb 11/2 gc/ms Inst : GC/MS 209 Mise 2 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112601.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 1,4-Dichlorobenzene-d4 Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 11.56 0.60 ug/1 167103 1,4-Dichlorobenzene-d4 11.70 Hit# Of 5 Tentative ID MW MolForm CAS# Qual
1 1,4-Dichlorobenzene-d4 150 C6C12D4 003855-82-1 72 2 Benzene-1,2<3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 43 3 Benzaldehyde, 2-hydroxy-3-methoxy- 152 C8H803 000148-53-8 10 4 Acenaphthylene 152 C12H8 000208-96-8 9 Abundance 4 Scan 710 (11,564 min): LBD.D (-) ~ m/z 149.90 100.00% 150
5000 115 52 78 38 1120 11.40 11.60 11.80 I 87 . 63 mti-> mmmm HTmTt 207 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 200 210 111'" ‘ i1''11'' ■' i ■ ■" i ■' • m/z 151.90 57.03% Abundance #9593:1,4-Dichlorobenzene-d4 150
5000 115 --TP —— --- 78 11 20 11.40 11,60 11.80 52 m/z 114.90 37.67% 35 87 miz-> 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 200 210 Abundance #9592: Benzene-1,2,3,4-d4-, 5,6-dichloro- 150
115 11,20 11,40 11,60 11.80 5000 52 78 m/z 78.05 20.51%
35 87
miz-> I ’71111 "’01111 I '" I ■ ■" ITT i'11' lmmmm m 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 200 210 Abundance #66892: Benzaldehyde, 2-hydroxy-3-methoxy- ------- — P 152 11.20 11,40 11,60 11.80 m/z52.00 17.47% 106 5000 53 81
122 । 1111" " I'1 1' i' ■'' i'' ‘' i mm 92 ll... 1136....1 ''111 n ' |'''' | ■''' |'''' |'' ‘ ‘ |'' ■ m/z—> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 11.20 1140 11.60 11.80.....
LBD.D NP112601.M Mon Dec 03 09:46:02 2001 Page 3
NYC-WTC_000030931
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NYC-WTC_000031054
Log sheet detailing sample preparation metrics for Method 608 analysis of WTC samples conducted in December 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069030
Calibration record for GC/MS instrument using TCLP method, listing standard compounds and response data from November 6, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069732
Calibration table listing standard compounds and response values for GCMS analysis dated November 16, 2001.
1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069271
Calibration data for GC/MS analysis including naphthalene and phenanthrene standards dated November 6, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000068815
Calibration data sheet for GC/MS instrument listing standards like naphthalene-d8 used for testing on November 6, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000087447
Calibration table and chromatographic data for the TCLP method using GC/MS instrument 209, dated October 4, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000067979
Calibration data table for GCMS TCLP analysis listing surrogate compounds and response factors from November 2, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000068230
Technical data sheet listing calibration standards and response factors for various polycyclic aromatic hydrocarbons.
1 shared non-person entities · 1 shared topics · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069349
Calibration data for GC/MS analysis including naphthalene and phenanthrene standards dated November 8, 2001.
1 shared topics · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069577
Calibration table data for GCMS analysis dated November 16-21, 2001, listing standard compounds and response values.
1 shared topics · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000068559
Calibration data table for GC/MS instrument used in TCLP analysis, generated on November 5, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000070089
DEP laboratory report documenting GC/MS results for sample AD25830 analyzed on December 6, 2001.
1 shared topics · similarity 0.991
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Gas chromatography-mass spectrometry scan record from early November to late December 2001 regarding environmental sample analysis.
Filed in the same folder
NYC-WTC_000030919
Log entry for GCMS scanning of World Trade Center environmental samples conducted in November 2001.
Filed in the same folder
NYC-WTC_000030933
Laboratory report documenting GCMS analysis of sample AD26079 conducted on December 3, 2001.
Filed in the same folder
NYC-WTC_000030944
Laboratory report documenting GCMS analysis of sample AD26080 conducted on December 3, 2001.
Filed in the same folder
NYC-WTC_000030955
Laboratory report documenting GCMS analysis of sample AD26127 conducted on December 3, 2001.
Filed in the same folder