Calibration data for GC/MS analysis using Method 508 and TCLP procedures dated November 30, 2001.
NYC-WTC_000030923–000030932Folder label: “GCMS SCAN X 11/2/01 AN 11/30/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV3001\LBD.D Vial: 51 Acq On : 30 Nov 2001 3:40 pm Operator: 209 GALOS Sample : lb 11/2 gc/ms Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Paramss LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112601.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 7.72 3.52 ug/1 980792 1,4-Dichlorobenzene-d4 11.70
Hit# Of 5 Tentative ID MW MolForm, CAS# Qual 1 2-Pentanone, 4-hydroxy-4-methyl- 116 C6H1202 000123-42-2 74 2 Acetic acid, ,1-dimethylethyl este 116 C6H1202 000540-88-5 25 3 Acetone / 58 C3H60 000067-64-1 16 4 5-Hexen-2-one 98 C6H10O 000109-49-9 9 Abundance ' Scan 291 (7.718 min): LBD.D (-) m/z 42.95 100.00% 43
5000 59
101 ' 7.40 7.60 7.80 8.00 0 , 69 83 mmmmml +pmm .......................................................... 207 m/z 59.05 43.65% T m/z-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #64275: 2-Pentanone, 4-hydroxy-4-methyl- 43
5000 "11 11111*1111*111’1’1 59 7.40 7.60 7.80 8.00 m/z 58.00 20.08% 15 31 . 101 - TTTTTIger 83 .1 miz-> 10 2030405060 70 8090 100 110 120 130 140 150 160 170 180 190 200210 Abundance #3292: Acetic acid, 1,1 -dimethylethyl ester 43 PT TRPT PP 7.40 7.60 7.80 8.00 5000 57 m/z 100.95 18.53% 101 15 27 Tppp + T l 11 U 1 1111 ||1, H . I| ||1.1. mz-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #62322: Acetone IIII TTRT PPP 43 7.40 7.60 7.80 8.00 m/z 41.05 6.82% 5000 58 27 _...... .lb..... 1...... UTTEEUUTTOTTITCUTCETETTCTEEE’TEEEIETETTETTTTITTITT ===== = 1 1 miz—> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 7.40 7.60 7.80 8.00
LBD.D NP112601.M Mon Dec 03 09:45:58 2001 Page 1
NYC-WTC_000030929
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NYC-WTC_000031054
Log sheet detailing sample preparation metrics for Method 608 analysis of WTC samples conducted in December 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069030
Calibration record for GC/MS instrument using TCLP method, listing standard compounds and response data from November 6, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069732
Calibration table listing standard compounds and response values for GCMS analysis dated November 16, 2001.
1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069271
Calibration data for GC/MS analysis including naphthalene and phenanthrene standards dated November 6, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000068815
Calibration data sheet for GC/MS instrument listing standards like naphthalene-d8 used for testing on November 6, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000087447
Calibration table and chromatographic data for the TCLP method using GC/MS instrument 209, dated October 4, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000067979
Calibration data table for GCMS TCLP analysis listing surrogate compounds and response factors from November 2, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000068230
Technical data sheet listing calibration standards and response factors for various polycyclic aromatic hydrocarbons.
1 shared non-person entities · 1 shared topics · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069349
Calibration data for GC/MS analysis including naphthalene and phenanthrene standards dated November 8, 2001.
1 shared topics · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069577
Calibration table data for GCMS analysis dated November 16-21, 2001, listing standard compounds and response values.
1 shared topics · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000068559
Calibration data table for GC/MS instrument used in TCLP analysis, generated on November 5, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000070089
DEP laboratory report documenting GC/MS results for sample AD25830 analyzed on December 6, 2001.
1 shared topics · similarity 0.991
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Gas chromatography-mass spectrometry scan record from early November to late December 2001 regarding environmental sample analysis.
Filed in the same folder
NYC-WTC_000030919
Log entry for GCMS scanning of World Trade Center environmental samples conducted in November 2001.
Filed in the same folder
NYC-WTC_000030933
Laboratory report documenting GCMS analysis of sample AD26079 conducted on December 3, 2001.
Filed in the same folder
NYC-WTC_000030944
Laboratory report documenting GCMS analysis of sample AD26080 conducted on December 3, 2001.
Filed in the same folder
NYC-WTC_000030955
Laboratory report documenting GCMS analysis of sample AD26127 conducted on December 3, 2001.
Filed in the same folder